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  Safety and Practical Aspects of Liquid-Phase Hydrogenation

Kennema, M., & Theyssen, N. (2015). Safety and Practical Aspects of Liquid-Phase Hydrogenation. In Catalytic Hydrogenation for Biomass Valorization (Chapter 13, pp. 282-298). London: Royal Society of Chemistry.

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 Creators:
Kennema, Marco1, Author              
Theyssen, Nils2, Author              
Affiliations:
1Research Group Rinaldi, Max-Planck-Institut für Kohlenforschung, Max Planck Society, ou_1445617              
2Service Department Theyssen (Technical Labs), Max-Planck-Institut für Kohlenforschung, Max Planck Society, ou_1445632              

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 Abstract: This chapter provides a description of necessary infrastructure for operation of lab-scale, high-pressure reactors. Furthermore, practical hints to improve the selection of the proper design and operation of a reactor vessel, with a focus on material selection and optimization concerning gas–liquid mass transport and heat removal, are discussed. The discussion is directed to improving reaction yields in order to approach the kinetic regime. For the risk assessment of liquid-phase hydrogenation, the hydrogen specific risks need to be considered, especially under the more severe reaction conditions, which are often required for conversion of biomass. Herein, a discussion of a variety of important safety parameters for the operation of larger autoclaves (≥ 500 mL), is given at an introductory level.

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Language(s): eng - English
 Dates: 2015
 Publication Status: Published in print
 Pages: -
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: DOI: 10.1039/9781782620099-00282
 Degree: -

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Title: Catalytic Hydrogenation for Biomass Valorization
Source Genre: Book
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Publ. Info: London : Royal Society of Chemistry, Chapter 13
Pages: - Volume / Issue: - Sequence Number: - Start / End Page: 282 - 298 Identifier: ISBN: 978-1-84973-801-9