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  N-oxides and related compounds. Part XL. Chemical and X-ray crystallographic investigation of the oxidation products of α-diketone bisacylhydrazones

Bauer, H., Boulton, A. J., Fedeli, W., Katrizky, A. R., Majid-Hamid, A., Mazza, F., et al. (1972). N-oxides and related compounds. Part XL. Chemical and X-ray crystallographic investigation of the oxidation products of α-diketone bisacylhydrazones. Journal of the Chemical Society-Perkin Transactions 2, 2(5), 662-667. doi:10.1039/P29720000662.

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Item Permalink: https://hdl.handle.net/11858/00-001M-0000-002D-8345-A Version Permalink: https://hdl.handle.net/11858/00-001M-0000-002D-8346-8
Genre: Journal Article

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JChemSocPekingTrans_2_1997_662.pdf (Any fulltext), 676KB
 
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http://pubs.rsc.org/en/content/articlepdf/1972/p2/p29720000662 (Any fulltext)
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https://doi.org/10.1039/P29720000662 (Any fulltext)
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 Creators:
Bauer, H1, Author           
Boulton, A. J., Author
Fedeli, W., Author
Katrizky, A. R., Author
Majid-Hamid, A., Author
Mazza, F., Author
Vagiago, A., Author
Affiliations:
1Department of Organic Chemistry, Max Planck Institute for Medical Research, Max Planck Society, ou_1497706              

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 Abstract: Oxidation of the title compounds yields O-acyl imidic acids derived from 1-amino-1,2,3-triazoles. This structure best explains the chemical and spectroscopic data and is confirmed by an X-ray crystallographic study of 1-(α-benzoyloxybenzylideneamino)-4,5-dimethyl-1,2,3-triazole (10). Crystals are monoclinic, space group P21/c with Z= 4 in a unit cell of dimensions: a= 5·94 ± 0·03, b= 10·76 ± 0·05, c= 27·31 ± 0·14 Å, β= 100·8°± 0·3°. The structure was solved by direct methods and refined to R 0·094.

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Language(s): eng - English
 Dates: 1971-09-301972
 Publication Status: Issued
 Pages: 6
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: DOI: 10.1039/P29720000662
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Title: Journal of the Chemical Society-Perkin Transactions 2
  Other : J. Chem. Soc.-Perkin Trans. 2
Source Genre: Journal
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Publ. Info: Cambridge, England : Royal Society of Chemistry
Pages: - Volume / Issue: 2 (5) Sequence Number: - Start / End Page: 662 - 667 Identifier: ISSN: 1472-779X
CoNE: https://pure.mpg.de/cone/journals/resource/111053443082010