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  A versatile liquid-jet setup for the European XFEL1

Schulz, J., Bielecki, J., Doak, B., Dörner, K., Graceffa, R., Shoeman, R. L., et al. (2019). A versatile liquid-jet setup for the European XFEL1. Journal of Synchrotron Radiation, 26(2), 339-345. doi:10.1107/S1600577519000894.

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JSynchrotronRad_26_2019_339.pdf (Any fulltext), 897KB
 
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 Creators:
Schulz, J., Author
Bielecki, J., Author
Doak, Bruce1, 2, Author           
Dörner, K., Author
Graceffa, R., Author
Shoeman, Robert L.1, 2, 3, Author           
Sikorski, M., Author
Thute, P., Author
Westphal, D., Author
Mancuso, A. P., Author
Affiliations:
1Department of Biomolecular Mechanisms, Max Planck Institute for Medical Research, Max Planck Society, ou_1497700              
2Coherent diffractive imaging, Max Planck Institute for Medical Research, Max Planck Society, ou_1497692              
3Analytical Protein Biochemistry, Max Planck Institute for Medical Research, Max Planck Society, ou_1497690              

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Free keywords: FEL physics, instrumentation, liquid jets, sample delivery
 Abstract: The SPB/SFX instrument of the European XFEL provides unique possibilities for high-throughput serial femtosecond crystallography. This publication presents the liquid-jet sample delivery setup of this instrument. The setup is compatible with state-of-the-art gas dynamic virtual nozzle systems as well as high-viscosity extruders and provides space and flexibility for other liquid injection devices and future upgrades. The liquid jets are confined in a differentially pumped catcher assembly and can be replaced within a couple of minutes through a load-lock. A two-microscope imaging system allows visual control of the jets from two perspectives.

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Language(s): eng - English
 Dates: 2018-11-072019-01-182019-03
 Publication Status: Issued
 Pages: 7
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Degree: -

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Title: Journal of Synchrotron Radiation
  Abbreviation : J. Synchrotron Radiat.
Source Genre: Journal
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Publ. Info: Copenhagen, Denmark : Published for the International Union of Crystallography by Munksgaard
Pages: - Volume / Issue: 26 (2) Sequence Number: - Start / End Page: 339 - 345 Identifier: ISSN: 1600-5775
ISSN: 0909-0495
CoNE: https://pure.mpg.de/cone/journals/resource/954925562624