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  Synthesis of polysarcosine from air and moisture stable N-phenoxycarbonyl-N-methylglycine assisted by tertiary amine base

Doriti, A., Brosnan, S. M., Weidner, S. M., & Schlaad, H. (2016). Synthesis of polysarcosine from air and moisture stable N-phenoxycarbonyl-N-methylglycine assisted by tertiary amine base. Polymer Chemistry, 7(18), 3067-3070. doi:10.1039/C6PY00221H.

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Item Permalink: https://hdl.handle.net/11858/00-001M-0000-002A-33D8-4 Version Permalink: https://hdl.handle.net/11858/00-001M-0000-002C-6085-D
Genre: Journal Article

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2265756.pdf (Publisher version), 321KB
 
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 Creators:
Doriti, Afroditi1, Author           
Brosnan, Sarah M.2, Author           
Weidner, Steffen M., Author
Schlaad, Helmut, Author
Affiliations:
1Davide Esposito, Kolloidchemie, Max Planck Institute of Colloids and Interfaces, Max Planck Society, ou_1863315              
2Helmut Schlaad, Kolloidchemie, Max Planck Institute of Colloids and Interfaces, Max Planck Society, ou_1863316              

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 Abstract: Polysarcosine (Mn = 3650-20 000 g mol-1, D [similar] 1.1) was synthesized from the air and moisture stable N-phenoxycarbonyl-N-methylglycine. Polymerization was achieved by in situ transformation of the urethane precursor into the corresponding N-methylglycine-N-carboxyanhydride, when in the presence of a non-nucleophilic tertiary amine base and a primary amine initiator.

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 Dates: 2016-04-082016-05-14
 Publication Status: Issued
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 Identifiers: DOI: 10.1039/C6PY00221H
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Title: Polymer Chemistry
  Abbreviation : Polym. Chem.
Source Genre: Journal
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Publ. Info: Cambridge, UK : Royal Society of Chemistry
Pages: - Volume / Issue: 7 (18) Sequence Number: - Start / End Page: 3067 - 3070 Identifier: ISSN: 1759-9954