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Abstract:
Direct fluorination of cyclic 1,3-diones gives 2-mono- and 2,2-di-fluorinated products. The monofluorinated compounds crystallise in their enol forms and the difluorinated compounds form stable monohydrates whose crystal structures have been elucidated. Direct fluorination of
phloroglucinol 1 in formic acid yields l,1,3,3,5,5-hexafluoro-2,2,4,4,6,6-hexahydroxycyclohexane.