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  Measurements of motionally averaged heteronuclear dipolar couplings in MAS NMR using R-type recoupling

Dvinskikh, S. V., Zimmermann, H., Maliniak, A., & Sandström, D. (2004). Measurements of motionally averaged heteronuclear dipolar couplings in MAS NMR using R-type recoupling. Journal of Magnetic Resonance, 168(2), 194-201. doi:10.1016/j.jmr.2004.03.001.

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Item Permalink: https://hdl.handle.net/11858/00-001M-0000-002A-1650-9 Version Permalink: https://hdl.handle.net/11858/00-001M-0000-002A-1651-7
Genre: Journal Article
Alternative Title : Measurements of motionally averaged heteronuclear dipolar couplings in MAS NMR using R-type recoupling

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JMagnReson_168_2004_194.pdf (Any fulltext), 287KB
 
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Dvinskikh, Sergey V., Author
Zimmermann, Herbert1, Author           
Maliniak, Arnold, Author
Sandström, Dick, Author
Affiliations:
1Emeritus Group Biophysics, Max Planck Institute for Medical Research, Max Planck Society, ou_1497712              

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Free keywords: Heteronuclear recoupling; Magic-angle spinning; SLF; PDLF; R-type sequences
 Abstract: A novel MAS NMR approach is presented for the determination of heteronuclear dipolar couplings in unoriented materials. The technique is based on the proton-detected local field (PDLF) protocol, and achieves dipolar recoupling by R-type radio-frequency irradiation. The experiment, which is called R-PDLF spectroscopy, is demonstrated on solid and liquid-crystalline systems. For mobile systems, it is shown that the R-PDLF scheme provides better dipolar resolution as compared to techniques combining conventional separated local field (SLF) spectroscopy with R-type recoupling.

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Language(s): eng - English
 Dates: 2004-04-052003-12-022004-04-092004-04-092004-06-01
 Publication Status: Issued
 Pages: 8
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: eDoc: 665900
DOI: 10.1016/j.jmr.2004.03.001
URI: http://www.ncbi.nlm.nih.gov/pubmed/15140427
URI: http://www.sciencedirect.com/science/article/pii/S1090780704000564
Other: 5971
 Degree: -

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Title: Journal of Magnetic Resonance
Source Genre: Journal
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Publ. Info: San Diego [etc.] : Academic Press
Pages: - Volume / Issue: 168 (2) Sequence Number: - Start / End Page: 194 - 201 Identifier: ISSN: 1090-7807 (Print)
CoNE: https://pure.mpg.de/cone/journals/resource/954922651175_1