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  Application of a novel directing effect in an organocopper/orthoester reaction to the synthesis of deuterium labeled unsaturated esters

Shattuck, J. C., Svatoš, A., Blazey, C. M., & Meinwald, J. (1997). Application of a novel directing effect in an organocopper/orthoester reaction to the synthesis of deuterium labeled unsaturated esters. Tetrahedron Letters, 38(39), 6803-6806. doi:10.1016/S0040-4039(97)01599-2.

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Shattuck, James C., Author
Svatoš, Aleš1, Author           
Blazey, Charles M., Author
Meinwald, Jerrold, Author
Affiliations:
1Research Group Mass Spectrometry, MPI for Chemical Ecology, Max Planck Society, ou_421899              

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 Abstract: A new short and highly flexible pathway to derivatives 3a-d and 5 dihydro-12-oxo-phytodienoic acid, using an electrochemical CC bond coupling in an one-step procedure, is described. Jasmonic acid can be coupled with carboxylic acids in a mixed Kolbe electrolysis in acceptable yields. Functional groups are tolerated and, hence, the method offers a simple route to the title compounds which are otherwise difficult to prepare.

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 Dates: 1997
 Publication Status: Issued
 Pages: -
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 Table of Contents: -
 Rev. Type: -
 Identifiers: Other: MS053
DOI: 10.1016/S0040-4039(97)01599-2
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Title: Tetrahedron Letters
  Other : Tetrahedron Lett.
Source Genre: Journal
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Publ. Info: Oxford : Pergamon
Pages: - Volume / Issue: 38 (39) Sequence Number: - Start / End Page: 6803 - 6806 Identifier: ISSN: 0040-4039
CoNE: https://pure.mpg.de/cone/journals/resource/954925448772