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  Facile Template Synthesis of Ordered Mesoporous Carbon with Polypyrrole as Carbon Precursor

Yang, C.-M., Weidenthaler, C., Spliethoff, B., Mamatha, M., & Schüth, F. (2005). Facile Template Synthesis of Ordered Mesoporous Carbon with Polypyrrole as Carbon Precursor. Chemistry of Materials, 17(2), 355-358. doi:10.1021/cm049164v.

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 Creators:
Yang, Chia-Min1, 2, Author           
Weidenthaler, Claudia1, Author           
Spliethoff, Bernd3, Author           
Mamatha, Mayanna1, Author           
Schüth, Ferdi1, Author           
Affiliations:
1Research Department Schüth, Max-Planck-Institut für Kohlenforschung, Max Planck Society, ou_1445589              
2Department of Chemistry, National Tsing Hua University , Hsinchu 30013, Taiwan, ou_persistent22              
3Service Department Tesche (EM), Max-Planck-Institut für Kohlenforschung, Max Planck Society, ou_1445631              

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 Abstract: A new and facile synthetic route of ordered mesoporous carbon with polypyrrole as carbon precursor has been developed. The mesoporous silica host is first impregnated with ferric chloride, which serves as the oxidant for the vapor-phase oxidative polymerization of pyrrole vapor at room temperature. Such a stoichiometric reaction provides a rational control of loading with polypyrrole and also determines the amount of carbon after subsequent pyrolysis in the host silica. Ordered mesoporous carbon is obtained after the dissolution of silica and iron species. The materials thus prepared have ordered structure, large surface area, and pore volume. They are ordered on the mesoscopic scale and show some graphitic order on the atomic scale.

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Language(s): eng - English
 Dates: 2004-05-262004-12-042005-01-01
 Publication Status: Published in print
 Pages: 4
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: DOI: 10.1021/cm049164v
 Degree: -

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Title: Chemistry of Materials
  Abbreviation : Chem. Mater.
Source Genre: Journal
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Publ. Info: Washington, D.C. : American Chemical Society
Pages: - Volume / Issue: 17 (2) Sequence Number: - Start / End Page: 355 - 358 Identifier: ISSN: 0897-4756
CoNE: https://pure.mpg.de/cone/journals/resource/954925561571