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  Wet Chemistry Synthesis of β‐Nickel Aluminide NiAl

Bönnemann, H., Brijoux, W., Hofstadt, H.-W., Ould-Ely, T., Schmidt, W., Waßmuth, B., et al. (2002). Wet Chemistry Synthesis of β‐Nickel Aluminide NiAl. Angewandte Chemie International Edition, 41(4), 599-603. doi:10.1002/1521-3773(20020215)41:4<599:AID-ANIE599>3.0.CO;2-R.

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 Creators:
Bönnemann, Helmut1, Author           
Brijoux, Werner1, Author           
Hofstadt, Hans-Werner2, Author           
Ould-Ely, Teyeb1, Author           
Schmidt, Wolfgang3, Author           
Waßmuth, Bernd4, Author           
Weidenthaler, Claudia3, Author           
Affiliations:
1Research Group Bönnemann, Max-Planck-Institut für Kohlenforschung, Max Planck Society, ou_1445600              
2Research Group Palkovits, Max-Planck-Institut für Kohlenforschung, Max Planck Society, ou_1445615              
3Research Department Schüth, Max-Planck-Institut für Kohlenforschung, Max Planck Society, ou_1445589              
4Service Department Mynott (NMR), Max-Planck-Institut für Kohlenforschung, Max Planck Society, ou_1445627              

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Free keywords: aluminum; intermetallic phases; metal-metal interactions; nickel; solid-state structures
 Abstract: A fine powder of β‐nickel aluminide NiAl is obtained by reaction of [Ni(cod)2] (cod=cycloocta‐1,5‐diene) with AlEt3 in toluene at room temperature and under a H2 pressure of 5–10 MPa and subsequent distillation of the solvent, subsequent hydrogenation (0.1–5 MPa), and annealing (200°C) [Eq. (a)]. This novel wet chemistry synthesis of aluminides may be transferred to Ni3Al (α‐nickel aluminide) and ternary aluminide powders such as GaNiAl, FeNiAl, and CeNiAl.

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Language(s): eng - English
 Dates: 2001-08-032002-02-142002-02-15
 Publication Status: Published in print
 Pages: 5
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Degree: -

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Title: Angewandte Chemie International Edition
  Abbreviation : Angew. Chem., Int. Ed.
Source Genre: Journal
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Publ. Info: Weinheim : Wiley-VCH
Pages: - Volume / Issue: 41 (4) Sequence Number: - Start / End Page: 599 - 603 Identifier: ISSN: 1433-7851
CoNE: https://pure.mpg.de/cone/journals/resource/1433-7851