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  Monomeric Sn(II) and Ge(II) hydrides supported by a tridentate pincer-based ligand

Khan, S., Samuel, P. P., Reent, M., Dieterich, J. M., Mata, R. A., Demers, J. P., et al. (2012). Monomeric Sn(II) and Ge(II) hydrides supported by a tridentate pincer-based ligand. Chemical communications, 48(40), 4890-4892. doi:10.1039/c2cc31214j.

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Item Permalink: https://hdl.handle.net/11858/00-001M-0000-000F-9DDA-6 Version Permalink: https://hdl.handle.net/11858/00-001M-0000-0029-C44B-F
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 Creators:
Khan, S., Author
Samuel, P. P., Author
Reent, M., Author
Dieterich, J. M., Author
Mata, R. A., Author
Demers, J. P.1, Author
Lange, A.1, Author
Roesky, H. W. , Author
Stalke, D., Author
Affiliations:
1Research Group of Solid-State NMR, MPI for Biophysical Chemistry, Max Planck Society, Göttingen, DE, ou_persistent35              

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 Abstract: Herein we report the syntheses of terminal Sn(II) (3) and Ge(II) (4) hydrides from the corresponding chloride precursors [{2,6-iPr2C6H3NCMe}2C6H3MCl] (M = Sn (1), Ge (2)) using [K{B(sec-Bu)3}H] as a hydrogenating agent. Combination of steric shielding and intramolecular N → M interactions resulted in the protection of M(II)–H bonds.

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Language(s): eng - English
 Dates: 2012-03-142012
 Publication Status: Issued
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 Table of Contents: -
 Rev. Type: Peer
 Identifiers: DOI: 10.1039/c2cc31214j
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Title: Chemical communications
Source Genre: Journal
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Pages: - Volume / Issue: 48 (40) Sequence Number: - Start / End Page: 4890 - 4892 Identifier: -