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  Experimental validation of a new integrated simulated moving bed process for the production of single enantiomers

García Palacios, J., Kramer, B., Kienle, A., & Kaspereit, M. (2011). Experimental validation of a new integrated simulated moving bed process for the production of single enantiomers. Journal of Chromatography A, 2218(16), 2232-2239. doi:10.1016/j.chroma.2011.02.021.

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Item Permalink: http://hdl.handle.net/11858/00-001M-0000-0013-8D0C-7 Version Permalink: http://hdl.handle.net/11858/00-001M-0000-0019-8D62-6
Genre: Journal Article

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 Creators:
García Palacios, J.1, 2, Author              
Kramer, Bernhard3, Author              
Kienle, A.1, 4, Author              
Kaspereit, M.1, Author              
Affiliations:
1Process Synthesis and Process Dynamics, Max Planck Institute for Dynamics of Complex Technical Systems, Max Planck Society, ou_1738153              
2International Max Planck Research School (IMPRS), Max Planck Institute for Dynamics of Complex Technical Systems, Max Planck Society, ou_1738143              
3Analysis and Redesign of Biological Networks, Max Planck Institute for Dynamics of Complex Technical Systems, Max Planck Society, ou_1738139              
4Otto-von-Guericke-Universität Magdeburg, External Organizations, ou_1738156              

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Free keywords: Simulated moving bed Enantiomer Racemization Gradient Integrated process Reactive separation
 Abstract: A new integrated 3-zone simulated moving bed (SMB) concept with internal racemization reaction was suggested recently for the production of single enantiomers from racemic mixtures [1,2]. The process utilizes an internal gradient to trigger the racemization within a single zone. It can deliver the pure enantiomer and outperforms conventional technologies. In this contribution, the concept is validated experimentally for the separation of a model system compound. The results demonstrate that the new concept is capable of producing a single enantiomer with purity, yield and conversion of 100%. © 2011 Elsevier B.V. All rights reserved. [accessed 2013 July 2nd]

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Language(s): eng - English
 Dates: 2011
 Publication Status: Published in print
 Pages: -
 Publishing info: -
 Table of Contents: -
 Rev. Method: Peer
 Identifiers: eDoc: 529954
Other: 9/11
DOI: 10.1016/j.chroma.2011.02.021
 Degree: -

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Title: Journal of Chromatography A
Source Genre: Journal
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Publ. Info: Amsterdam : Elsevier
Pages: - Volume / Issue: 2218 (16) Sequence Number: - Start / End Page: 2232 - 2239 Identifier: ISSN: 0021-9673
CoNE: /journals/resource/954925527837_1