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  Optimal Design of Experiments for Parameter Identification of Ceramic Porous Membranes

Zhang, F., Mangold, M., & Kienle, A. (2009). Optimal Design of Experiments for Parameter Identification of Ceramic Porous Membranes. Chemical Engineering and Technology, 32(4), 641-649. doi:10.1002/ceat.200800544.

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Item Permalink: http://hdl.handle.net/11858/00-001M-0000-0013-935D-B Version Permalink: http://hdl.handle.net/11858/00-001M-0000-0014-BD95-1
Genre: Journal Article

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 Creators:
Zhang, F.1, Author              
Mangold, M.1, Author              
Kienle, A.1, 2, Author              
Affiliations:
1Process Synthesis and Process Dynamics, Max Planck Institute for Dynamics of Complex Technical Systems, Max Planck Society, ou_1738153              
2Otto-von-Guericke-Universität Magdeburg, External Organizations, ou_1738156              

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 Abstract: Six different experimental schemes for mass transfer through porous membranes are compared for the efficiency with respect to parameter identification, namely dynamic single-gas permeation, dynamic multi-gas permeation, steady state single-gas permeation, steady state multi-gas permeation, transient diffusion and isobaric diffusion experiments. The comparison is made under optimal experimental conditions, which is obtained from optimal experimental design (OED) based on the Fisher information matrix. The covariance matrix of the parameters for each experimental scheme is estimated by the Cramér-Rao lower bound. To solve the optimization problems, a hybrid optimizer which combines a genetic algorithm and a gradient based algorithm is used. Copyright © 2009 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim [accessed April 22, 2009]

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Language(s): eng - English
 Dates: 2009
 Publication Status: Published in print
 Pages: -
 Publishing info: -
 Table of Contents: -
 Rev. Method: -
 Identifiers: eDoc: 429161
DOI: 10.1002/ceat.200800544
Other: 5/09
 Degree: -

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Title: Chemical Engineering and Technology
Source Genre: Journal
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Publ. Info: New York : J. Wiley
Pages: - Volume / Issue: 32 (4) Sequence Number: - Start / End Page: 641 - 649 Identifier: ISSN: 0930-7516
CoNE: /journals/resource/991042744467904