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  Feasibility Studies and Dynamics of Catalytic Liquid Phase Esterification Reactions in a Micro Plant

Kulkarni, A. A., Zeyer, K. P., Jacobs, T., Kaspereit, M., & Kienle, A. (2008). Feasibility Studies and Dynamics of Catalytic Liquid Phase Esterification Reactions in a Micro Plant. Chemical Engineering Journal, 135(Suppl. 1), S270-S275. doi:10.1016/j.cej.2007.07.024.

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Item Permalink: http://hdl.handle.net/11858/00-001M-0000-0013-9667-1 Version Permalink: http://hdl.handle.net/11858/00-001M-0000-0028-1464-B
Genre: Journal Article

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 Creators:
Kulkarni, A. A.1, Author              
Zeyer, K. P.2, Author              
Jacobs, T.2, Author
Kaspereit, M.2, Author              
Kienle, A.2, 3, Author              
Affiliations:
1National Chemical Laboratory, Pune, India., persistent:22              
2Process Synthesis and Process Dynamics, Max Planck Institute for Dynamics of Complex Technical Systems, Max Planck Society, ou_1738153              
3Otto-von-Guericke-Universität Magdeburg, External Organizations, ou_1738156              

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 Abstract: We present a new micro reactor concept which is suitable for investigations of heterogeneously catalyzed liquid phase reactions. In the set-up two reactants are mixed in a commercially available interdigital micro mixer. The outlet of the micro mixer is connected to a modular micro reactor that consists of stacked plates. Each plate contains a milled meandering channel filled with catalyst beads. By using a variable number of plates the residence time can be manipulated and thus adjusted for a specific task. The synthesis of butyl acetate is considered as a model reaction since it has been investigated in detail in conventional reaction systems. In a first step, some experimental results of the heterogeneously catalyzed reaction are presented. In the second part, the set-up is operated as a chromatographic reactor. Dynamic behaviour is investigated applying the elution chromatography mode and the frontal analysis mode. Copyright © 2007 Elsevier B.V. All rights reserved. [accessed May 28, 2008]

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Language(s): eng - English
 Dates: 2008
 Publication Status: Published in print
 Pages: -
 Publishing info: -
 Table of Contents: -
 Rev. Method: -
 Identifiers: eDoc: 298161
Other: 10/08
DOI: 10.1016/j.cej.2007.07.024
 Degree: -

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Title: Chemical Engineering Journal
Source Genre: Journal
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Publ. Info: Lausanne : Elsevier
Pages: - Volume / Issue: 135 (Suppl. 1) Sequence Number: - Start / End Page: S270 - S275 Identifier: ISSN: 1385-8947
CoNE: https://pure.mpg.de/cone/journals/resource/954925622211