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  Application of an eremomycin-chiral stationary phase for the separation of DL-methionine using simulated moving bed technology

Zhang, L., Gedicke, K., Kuznetsov, M. A., Staroverov, S. M., & Seidel-Morgenstern, A. (2007). Application of an eremomycin-chiral stationary phase for the separation of DL-methionine using simulated moving bed technology. Journal of Chromatography A, 1162, 90-96. doi:10.1016/j.chroma.2007.04.033.

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Zhang, L.1, Autor           
Gedicke, K.1, Autor           
Kuznetsov, M. A.2, Autor
Staroverov, S. M.2, Autor
Seidel-Morgenstern, A.1, 3, Autor           
Affiliations:
1Physical and Chemical Foundations of Process Engineering, Max Planck Institute for Dynamics of Complex Technical Systems, Max Planck Society, ou_1738150              
2Lomonosov State University, Chemistry Department, Russian Federation, ou_persistent22              
3Otto-von-Guericke-Universität Magdeburg, External Organizations, ou_1738156              

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Schlagwörter: eremomycin; chiral stationary phase; methionine; simulated moving bed; adsorption isotherms; stability
 Zusammenfassung: Recently a new chiral stationary phase (CSP) was introduced, based on the immobilization of the macrocyclic glycopeptide eremomycin to epoxy-activated silica. The application of this new CSP to preparative enantioseparation using simulated moving bed chromatography (SMB) will be presented. In such delicate continuous separation processes, besides selectivity, the long-term stability of the applied stationary phases is of importance. Column to column fluctuations of the bed homogeneity and long-term stability of the preparative stationary phase was satisfactory according to the results of perturbation experiments performed before and after long-term SMB runs. Copyright © 2007 Elsevier B.V. All rights reserved. [accessed 2013 November 26th]

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Sprache(n): eng - English
 Datum: 2007
 Publikationsstatus: Erschienen
 Seiten: -
 Ort, Verlag, Ausgabe: -
 Inhaltsverzeichnis: -
 Art der Begutachtung: -
 Identifikatoren: eDoc: 298326
DOI: 10.1016/j.chroma.2007.04.033
 Art des Abschluß: -

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Titel: Journal of Chromatography A
Genre der Quelle: Zeitschrift
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Ort, Verlag, Ausgabe: Amsterdam : Elsevier
Seiten: - Band / Heft: 1162 Artikelnummer: - Start- / Endseite: 90 - 96 Identifikator: ISSN: 0021-9673
CoNE: https://pure.mpg.de/cone/journals/resource/954925527837_1