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  Application of an eremomycin-chiral stationary phase for the separation of DL-methionine using simulated moving bed technology

Zhang, L., Gedicke, K., Kuznetsov, M. A., Staroverov, S. M., & Seidel-Morgenstern, A. (2007). Application of an eremomycin-chiral stationary phase for the separation of DL-methionine using simulated moving bed technology. Journal of Chromatography A, 1162, 90-96. doi:10.1016/j.chroma.2007.04.033.

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Item Permalink: http://hdl.handle.net/11858/00-001M-0000-0013-98BE-D Version Permalink: http://hdl.handle.net/11858/00-001M-0000-0014-B6B5-D
Genre: Journal Article

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 Creators:
Zhang, L.1, Author              
Gedicke, K.1, Author              
Kuznetsov, M. A.2, Author
Staroverov, S. M.2, Author
Seidel-Morgenstern, A.1, 3, Author              
Affiliations:
1Physical and Chemical Foundations of Process Engineering, Max Planck Institute for Dynamics of Complex Technical Systems, Max Planck Society, ou_1738150              
2Lomonosov State University, Chemistry Department, Russian Federation, ou_persistent22              
3Otto-von-Guericke-Universität Magdeburg, External Organizations, ou_1738156              

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Free keywords: eremomycin; chiral stationary phase; methionine; simulated moving bed; adsorption isotherms; stability
 Abstract: Recently a new chiral stationary phase (CSP) was introduced, based on the immobilization of the macrocyclic glycopeptide eremomycin to epoxy-activated silica. The application of this new CSP to preparative enantioseparation using simulated moving bed chromatography (SMB) will be presented. In such delicate continuous separation processes, besides selectivity, the long-term stability of the applied stationary phases is of importance. Column to column fluctuations of the bed homogeneity and long-term stability of the preparative stationary phase was satisfactory according to the results of perturbation experiments performed before and after long-term SMB runs. Copyright © 2007 Elsevier B.V. All rights reserved. [accessed 2013 November 26th]

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Language(s): eng - English
 Dates: 2007
 Publication Status: Published in print
 Pages: -
 Publishing info: -
 Table of Contents: -
 Rev. Method: -
 Identifiers: eDoc: 298326
DOI: 10.1016/j.chroma.2007.04.033
 Degree: -

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Title: Journal of Chromatography A
Source Genre: Journal
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Publ. Info: Amsterdam : Elsevier
Pages: - Volume / Issue: 1162 Sequence Number: - Start / End Page: 90 - 96 Identifier: ISSN: 0021-9673
CoNE: https://pure.mpg.de/cone/journals/resource/954925527837_1