Deutsch
 
Hilfe Datenschutzhinweis Impressum
  DetailsucheBrowse

Datensatz

DATENSATZ AKTIONENEXPORT
  Production of Butyl Acetate by Catalytic Distillation : Theoretical and Experimental Studies

Singh, A., Hiwale, R., Mahajani, S. M., Gudi, R. D., Gangadwala, J., & Kienle, A. (2005). Production of Butyl Acetate by Catalytic Distillation: Theoretical and Experimental Studies. Industrial and Engineering Chemistry Research, 44(9), 3042-3052. doi:10.1021/ie049659u.

Item is

Externe Referenzen

einblenden:

Urheber

einblenden:
ausblenden:
 Urheber:
Singh, A.1, Autor
Hiwale, R.1, Autor
Mahajani, S. M.1, Autor
Gudi, R. D.1, Autor
Gangadwala, J.2, Autor           
Kienle, A.2, 3, Autor           
Affiliations:
1Department of Chemical Engineering, Indian Institute of Technology, Bombay, Mumbai, India, ou_persistent22              
2Process Synthesis and Process Dynamics, Max Planck Institute for Dynamics of Complex Technical Systems, Max Planck Society, ou_1738153              
3Otto-von-Guericke-Universität Magdeburg, External Organizations, ou_1738156              

Inhalt

einblenden:
ausblenden:
Schlagwörter: -
 Zusammenfassung: The esterification reaction of acetic acid with n-butanol in a continuous catalytic distillation system has been studied. The products of esterification reactions viz, water and butyl acetates are separated by distillation during the course of the reaction, to overcome the equilibrium limitations. A 3-m-tall column with reactive and nonreactive zones, packed with a commercial catalytic packing (KATAPAK-S) and noncatalytic wire gauze packing, was used for this purpose. For a feed concentration corresponding to that obtained in a one-stage continuously stirred tank reactor at reaction equilibrium, conversion of ~100% was realized, with selectivity on the order of 99%. Interestingly, in most of the experiments, the bottom stream contained butyl acetate that was almost free of acetic acid. The influence of various operating parameters, such as feed flow rate, feed composition, feed location, and boil-up rate, on the conversion, selectivity, and separation was studied. A dynamic equilibrium stage model was developed and solved to predict the transient and steady-state results. Reasonably good agreement between the experimental and simulation results was realized. © 2005 American Chemical Society. [accessed 2014 January 9th]

Details

einblenden:
ausblenden:
Sprache(n): eng - English
 Datum: 2005
 Publikationsstatus: Erschienen
 Seiten: -
 Ort, Verlag, Ausgabe: -
 Inhaltsverzeichnis: -
 Art der Begutachtung: Expertenbegutachtung
 Identifikatoren: eDoc: 217656
Anderer: 6/05
DOI: 10.1021/ie049659u
 Art des Abschluß: -

Veranstaltung

einblenden:

Entscheidung

einblenden:

Projektinformation

einblenden:

Quelle 1

einblenden:
ausblenden:
Titel: Industrial and Engineering Chemistry Research
Genre der Quelle: Zeitschrift
 Urheber:
Affiliations:
Ort, Verlag, Ausgabe: Washington, D.C : American Chemical Society
Seiten: - Band / Heft: 44 (9) Artikelnummer: - Start- / Endseite: 3042 - 3052 Identifikator: ISSN: 0888-5885
CoNE: https://pure.mpg.de/cone/journals/resource/954928546246