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  Singular Points of Reactive Distillation Systems

Qi, Z., Flockerzi, D., & Sundmacher, K. (2004). Singular Points of Reactive Distillation Systems. AIChE Journal, 50, 2866-2876. doi:10.1002/aic.10259.

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Item Permalink: http://hdl.handle.net/11858/00-001M-0000-0013-9E93-A Version Permalink: http://hdl.handle.net/11858/00-001M-0000-002C-8A1F-3
Genre: Journal Article

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flocke_rev_manu_1757835.pdf (Postprint), 95KB
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flocke_figures_1757835.pdf (Postprint), 93KB
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This publication is with permission of the rights owner freely accessible due to an Alliance license and a national license (funded by the DFG, German Research Foundation) respectively
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 Creators:
Qi, Zhiwen1, Author              
Flockerzi, D.2, Author              
Sundmacher, Kai1, 3, Author              
Affiliations:
1Process Systems Engineering, Max Planck Institute for Dynamics of Complex Technical Systems, Max Planck Society, ou_1738151              
2Systems and Control Theory, Max Planck Institute for Dynamics of Complex Technical Systems, Max Planck Society, ou_1738154              
3Otto-von-Guericke-Universität Magdeburg, External Organizations, ou_1738156              

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 Abstract: For the conceptual design of countercurrently operated reactive distillation columns, fast methods are needed to estimate potential top and bottom products. The possible column bottom product composition can be determined from the stable singular points of a batch reactive reboiler. In a similar manner the top product composition can be obtained from the stable singular points of a batch reactive condenser. Geometrically, the singular points of both batch processes are located on a common potential singular point surface (PSPS) whose trajectory depends on the reaction stoichiometry and the phase equilibria. At the singular points, the PSPS intersects a reaction kinetic surface that is dependent on the reaction rate expression and the phase equilibrium of a reference component. Based on the singularity analysis, a single-feed reactive distillation column can be designed. Several hypothetical and real reaction systems are analyzed to illustrate the singularity analysis and the design procedure. Copyright © 1999–2013 John Wiley & Sons, Inc. All Rights Reserved. [accessed 2013 August 15th]

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Language(s): eng - English
 Dates: 2004
 Publication Status: Published in print
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 Rev. Method: Peer
 Identifiers: DOI: 10.1002/aic.10259
Other: 30/04
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Title: AIChE Journal
Source Genre: Journal
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Pages: - Volume / Issue: 50 Sequence Number: - Start / End Page: 2866 - 2876 Identifier: -