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  Solubility measurement using differential scanning calorimetry

Mohan, R., Lorenz, H., & Myerson, A. S. (2002). Solubility measurement using differential scanning calorimetry. Industrial and Engineering Chemistry Research, 41(19), 4854-4862. doi:10.1021/ie0200353.

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Item Permalink: http://hdl.handle.net/11858/00-001M-0000-0013-A071-3 Version Permalink: http://hdl.handle.net/11858/00-001M-0000-0014-BA4F-6
Genre: Journal Article
Alternative Title : Ind. Eng. Chem. Res.

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 Creators:
Mohan, R.1, Author
Lorenz, H.2, Author              
Myerson, A. S.3, Author
Affiliations:
1Andrx Pharmaceuticals, Fort Lauderdale, FL , United States , ou_persistent22              
2Physical and Chemical Foundations of Process Engineering, Max Planck Institute for Dynamics of Complex Technical Systems, Max Planck Society, ou_1738150              
3Department of Chemical Engineering, Illinois Institute of Technology, 103 Siegel Hall, 3301 South Dearborn Street, Chicago, ou_persistent22              

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 Abstract: The measurement of solubility in microsamples employing a differential scanning calorimeter (DSC) has been evaluated for several aqueous and nonaqueous systems substance A in acetonitrile, (RS) mandelic acid, (S) mandelic acid, adipic acid, diphenhydramine HCl, alpha glycine, and terephthalic acid in water, (RS)-mandelic acid and beta succinic acid in ethanol and methanol, and adipic acid in ethanol. This technique requires samples in the range of milligrams and can be used at high temperatures and pressures. Results show that the solubility data of most compounds studied using this technique are within 5% of solubility data obtained from the literature. Factors that influence solubility measurement by DSC were examined along with methods to minimize associated errors. Copyright © 2002 American Chemical Society [accessed 2013 November 29th]

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Language(s): eng - English
 Dates: 2002
 Publication Status: Published in print
 Pages: -
 Publishing info: -
 Table of Contents: -
 Rev. Method: Peer
 Identifiers: eDoc: 13785
DOI: 10.1021/ie0200353
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Title: Industrial and Engineering Chemistry Research
Source Genre: Journal
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Publ. Info: Washington, D.C : American Chemical Society
Pages: - Volume / Issue: 41 (19) Sequence Number: - Start / End Page: 4854 - 4862 Identifier: ISSN: 0888-5885
CoNE: /journals/resource/954928546246