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  A Rapid and Reliable Assay for Regioselectivity Using Fluorescence Spectroscopy

Angelovski, G., Keränen, M., Linnepe, P., Grudzielanek, S., & Eilbracht, P. (2006). A Rapid and Reliable Assay for Regioselectivity Using Fluorescence Spectroscopy. Advanced Synthesis & Catalysis, 348(10-11), 1193-1199. doi:10.1002/adsc.200606047.

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Item Permalink: http://hdl.handle.net/11858/00-001M-0000-0013-D0C9-4 Version Permalink: http://hdl.handle.net/21.11116/0000-0004-6FB5-4
Genre: Journal Article

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Angelovski, G1, Author              
Keränen, MD, Author
Linnepe, P, Author
Grudzielanek, S, Author
Eilbracht, P, Author
Affiliations:
1External Organizations, ou_persistent22              

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 Abstract: The first report of a fluorescence-based assay for the direct measurement of the regioselectivity of a reaction is described herein, developed from the desire to construct a quicker analytical method for the determination of the ratio of regioisomers obtained in the tandem hydroformylation/Fischer indole synthesis. The method allows for extremely rapid acquisition times, as the use of crude reaction mixtures is allowed. The assay is also shown to be overall very reliable, tolerating the presence of various functional groups and proceeding on average with a standard error of measurement comparable to that of NMR. As fluorescence is the only requirement for the employment of this analytical method, countless numbers of target-specific assays can undoubtedly be developed based upon this initial finding.

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 Dates: 2006-07
 Publication Status: Published in print
 Pages: -
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 Table of Contents: -
 Rev. Type: -
 Identifiers: DOI: 10.1002/adsc.200606047
BibTex Citekey: 4049
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Title: Advanced Synthesis & Catalysis
  Abbreviation : Adv. Synth. Catal.
Source Genre: Journal
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Publ. Info: Weinheim, Fed. Rep. of Germany : Wiley-VCH Verlag GmbH
Pages: - Volume / Issue: 348 (10-11) Sequence Number: - Start / End Page: 1193 - 1199 Identifier: ISSN: 1615-4150
CoNE: https://pure.mpg.de/cone/journals/resource/958634688013