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  Application of Immobilized Free Radicals in Supercritical Fluid Chromatography Hyphenated with Proton Nuclear Magnetic Resonance Spectroscopy

Fischer, H., Poggio T, Raitza, M., & Albert, K. (2000). Application of Immobilized Free Radicals in Supercritical Fluid Chromatography Hyphenated with Proton Nuclear Magnetic Resonance Spectroscopy. Magnetic Resonance in Chemistry, 38(5), 336-342. Retrieved from http://www3.interscience.wiley.com/cgi-bin/fulltext?ID=72503955PLACEBO=IE.pdf.

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Item Permalink: http://hdl.handle.net/11858/00-001M-0000-0013-E58B-5 Version Permalink: http://hdl.handle.net/11858/00-001M-0000-0013-E58C-3
Genre: Journal Article

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Fischer, HH1, Author              
Poggio T, Raitza, M, Author
Albert, K, Author
Affiliations:
1Max Planck Institute for Biological Cybernetics, Max Planck Society, ou_1497794              

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 Abstract: Immobilized free radicals were synthesized and used to shorten the spin-lattice relaxation times of analytes in the hyphenation of supercritical fluid chromatography (SFC) with proton high-field nuclear magnetic resonance spectroscopy (NMR). The effect of the immobilized free radicals was studied for the first time under on-line SFC-NMR coupling conditions. With this method it was possible to obtain integratable NMR spectra in on-line continuous-flow SFC-1H NMR spectroscopy.

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 Dates: 2000
 Publication Status: Published in print
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Title: Magnetic Resonance in Chemistry
Source Genre: Journal
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Pages: - Volume / Issue: 38 (5) Sequence Number: - Start / End Page: 336 - 342 Identifier: -