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Free keywords:
hydrothermal synthesis; M1 phase; MoVTeNb oxides; polyoxometalates; Raman spectroscopy
Abstract:
n situ Raman spectroscopy allows insight into molecular processes under hydrothermal conditions during synthesis of complex nanostructured MoVTeNb oxides (see picture: Nb yellow, Mo blue, V/Mo pale blue, Te red). Based on the knowledge acquired, the synthesis can be more efficiently directed towards the desired product with improved functionality.