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  The Haber–Bosch Process Revisited: On the Real Structure and Stability of “Ammonia Iron” under Working Condition

Kandemir, T., Schuster, M. E., Senyshyn, A., Behrens, M., & Schlögl, R. (2013). The Haber–Bosch Process Revisited: On the Real Structure and Stability of “Ammonia Iron” under Working Condition. Angewandte Chemie International Edition, 52(48), 12723-12726. doi:10.1002/anie.201305812.

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Item Permalink: https://hdl.handle.net/11858/00-001M-0000-0014-7C1F-6 Version Permalink: https://hdl.handle.net/21.11116/0000-000E-3AAE-E
Genre: Journal Article

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 Creators:
Kandemir, Timur1, Author           
Schuster, Manfred Erwin1, Author           
Senyshyn, Anatoliy2, Author
Behrens, Malte1, Author           
Schlögl, Robert1, Author           
Affiliations:
1Inorganic Chemistry, Fritz Haber Institute, Max Planck Society, ou_24023              
2Forschungsneutronenquelle Heinz Maier-Leibnitz (FRM II) Technische Universität München, Lichtenbergstrasse 1, 85747 Garching (Germany), ou_persistent22              

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Free keywords: catalyst microstructure;Haber–Bosch process;heterogeneous catalysis;iron nitridation;neutron diffraction
 Abstract: In situ neutron diffraction was used to study the structural properties of an industrial ammonia synthesis catalyst under working conditions similar to those of the Haber–Bosch process. Despite favorable thermodynamics, no indications of reversible bulk nitridation of the iron catalyst was observed in a self-generated ammonia concentration of 12 vol % at 425 °C and 75 bar after 88 h on stream.

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Language(s): eng - English
 Dates: 2013-07-042013-10-092013-11-25
 Publication Status: Issued
 Pages: 4
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: DOI: 10.1002/anie.201305812
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Title: Angewandte Chemie International Edition
  Abbreviation : Angew. Chem. Int. Ed.
Source Genre: Journal
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Publ. Info: Weinheim : Wiley-VCH
Pages: - Volume / Issue: 52 (48) Sequence Number: - Start / End Page: 12723 - 12726 Identifier: Other: 1433-7851
ISSN: 1521-3773
CoNE: https://pure.mpg.de/cone/journals/resource/0570-0833