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  SPS-assisted preparation of the Magnéli phase WO2.90 for thermoelectric applications

Kieslich, G., Birkel, C. S., Douglas, J. E., Gaultois, M., Veremchuk, I., Seshadri, R., et al. (2013). SPS-assisted preparation of the Magnéli phase WO2.90 for thermoelectric applications. Journal of Materials Chemistry A, 1(42), 13050-13054. doi:10.1039/c3ta12145c.

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Item Permalink: http://hdl.handle.net/11858/00-001M-0000-0015-1FC1-6 Version Permalink: http://hdl.handle.net/11858/00-001M-0000-0015-1FC2-4
Genre: Journal Article

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 Creators:
Kieslich, G., Author
Birkel, C. S., Author
Douglas, J. E., Author
Gaultois, M., Author
Veremchuk, I.1, Author              
Seshadri, R., Author
Stucky, G. D., Author
Grin, Y.2, Author              
Tremel, W., Author
Affiliations:
1Igor Veremchuk, Chemical Metal Science, Max Planck Institute for Chemical Physics of Solids, Max Planck Society, ou_1863411              
2Juri Grin, Chemical Metal Science, Max Planck Institute for Chemical Physics of Solids, Max Planck Society, ou_1863413              

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 Abstract: We describe the preparation and simultaneous consolidation of WO2.90 by spark plasma sintering (SPS). SPS allows for the direct manufacturing of large amounts of consolidated material. Synchrotron powder X-ray diffraction indicates that the material is single phase. Microstructure analysis indicates that the pellet is fully dense, allowing high-temperature thermoelectric properties to be reliably measured. The as-prepared samples of WO2.90 reach a ZT of 0.1 at 1100 K.

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 Dates: 2013
 Publication Status: Published in print
 Pages: -
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 Table of Contents: -
 Rev. Type: -
 Identifiers: eDoc: 671334
ISI: 000325577300003
DOI: 10.1039/c3ta12145c
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Title: Journal of Materials Chemistry A
Source Genre: Journal
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Pages: - Volume / Issue: 1 (42) Sequence Number: - Start / End Page: 13050 - 13054 Identifier: ISSN: 2050-7488