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  Solution conformation of the tetrasaccharide glycoside Xylβ1-(Manα1-3)2Manβ1-4Glcβ1R from the mollu-series glycosphingolipids

Dabrowski, U., Dabrowski, J., Grosskurth, H., Von der Lieth, C. W., & Ogawa, T. (1993). Solution conformation of the tetrasaccharide glycoside Xylβ1-(Manα1-3)2Manβ1-4Glcβ1R from the mollu-series glycosphingolipids. Biochemical and Biophysical Research Communications, 192(3), 1057-1065. doi:10.1006/bbrc.1993.1524.

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Item Permalink: https://hdl.handle.net/11858/00-001M-0000-0019-AA5C-1 Version Permalink: https://hdl.handle.net/11858/00-001M-0000-002D-224D-7
Genre: Journal Article
Alternative Title : Solution conformation of the tetrasaccharide glycoside Xylβ1-(Manα1-3)2Manβ1-4Glcβ1R from the mollu-series glycosphingolipids

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Dabrowski, Ursula1, Author           
Dabrowski, Janusz1, Author           
Grosskurth, Horst2, Author           
Von der Lieth, Claus Wilhelm, Author
Ogawa, Tomoya, Author
Affiliations:
1Department of Organic Chemistry, Max Planck Institute for Medical Research, Max Planck Society, ou_1497706              
2Department of Molecular Neurobiology, Max Planck Institute for Medical Research, Max Planck Society, ou_1497704              

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 Abstract: The conformation of Xylβ1-(Manα1-3)2Manβ1-4Glcβ1-OCH2CH(N3)CH(OH) CHCHC13H27 tetrasaccharide glycoside in Me2SO-d6 was investigated with use of a distance mapping procedure based on rotating-frame NOE and hydrogen bond constraints, and Molecular Mechanics calculations. The Manα1-3Manβ linkage was found to be well defined in a single conformation, whereas some flexibility could he assumed for the remaining two glycosidic linkages. Similar conclusions, though based on a smaller number of constraints, were drawn for the title compound anchored in mixed D2O/dodecylphosphocholine-d38 micelles.

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Language(s): eng - English
 Dates: 1993-03-161993-05-14
 Publication Status: Issued
 Pages: 9
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: eDoc: 665139
DOI: 10.1006/bbrc.1993.1524
Other: 6948
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Title: Biochemical and Biophysical Research Communications
  Other : Biochem. Biophys. Res. Commun.
Source Genre: Journal
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Publ. Info: Orlando, Fla. : Academic Press
Pages: - Volume / Issue: 192 (3) Sequence Number: - Start / End Page: 1057 - 1065 Identifier: ISSN: 0006-291X
CoNE: https://pure.mpg.de/cone/journals/resource/954922652205_1