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  ESR and ENDOR study of 2,3‐dihydro‐1‐oxo‐1λ4,2,3,5‐thiatriazol‐3‐yl radicals

Neugebauer, F. A. (1992). ESR and ENDOR study of 2,3‐dihydro‐1‐oxo‐1λ4,2,3,5‐thiatriazol‐3‐yl radicals. Magnetic Resonance in Chemistry, 30(1), 84-86. doi:10.1002/mrc.1260300117.

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Item Permalink: https://hdl.handle.net/11858/00-001M-0000-0019-ABB3-6 Version Permalink: https://hdl.handle.net/21.11116/0000-0002-553F-9
Genre: Journal Article

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MagResonChem_30_1992_84.pdf (Any fulltext), 193KB
 
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http://onlinelibrary.wiley.com/doi/10.1002/mrc.1260300117/epdf (Any fulltext)
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 Creators:
Neugebauer, Franz A.1, Author           
Affiliations:
1Department of Organic Chemistry, Max Planck Institute for Medical Research, Max Planck Society, ou_1497706              

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Free keywords: ESR; Nitrogen-centred radicals; 2,3-Dihydro-1-oxo-1λ4,2,3,5-thiatriazol-3-yl radicals
 Abstract: Dehydrogenation of 2,5‐dihydro‐1,2,3,5‐thiatriazole 1‐oxides with thermally formed bis(4‐methylphenyl)aminyl generated 2,3‐dihydro‐1‐oxo‐1λ4,2,3,5‐thiatriazol‐3‐yl radicals. ESR, ENDOR and triple resonance studies in combination with 15N labelling yielded the magnitude and assignment of all 1H and 14N hyperfine coupling (HFC) constants. The radicals have a basic five‐π‐electron amidrazon‐2‐yl structure with the highest spin density at N‐2.

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Language(s): eng - English
 Dates: 1991-03-181991-07-242005-04-121992-01-01
 Publication Status: Issued
 Pages: 3
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: DOI: 10.1002/mrc.1260300117
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Title: Magnetic Resonance in Chemistry
  Abbreviation : Magn. Reson. Chem.
Source Genre: Journal
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Publ. Info: Hoboken, N.Y., USA : John Wiley & Sons
Pages: - Volume / Issue: 30 (1) Sequence Number: - Start / End Page: 84 - 86 Identifier: ISSN: 0749-1581
CoNE: https://pure.mpg.de/cone/journals/resource/954928503544