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  Accurate metal and oxygen analyses of cuprate single crystals by electron probe microanalysis

Mackenzie, A. P. (1991). Accurate metal and oxygen analyses of cuprate single crystals by electron probe microanalysis. Physica C-Superconductivity and its Applications, 178(4-6), 365-376. doi:10.1016/0921-4534(91)90085-D.

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Item Permalink: http://hdl.handle.net/11858/00-001M-0000-0018-E802-2 Version Permalink: http://hdl.handle.net/11858/00-001M-0000-0018-E804-D
Genre: Journal Article

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Mackenzie, A. P.1, Author              
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 Abstract: Accurate knowledge of the stoichiometry of single crystals has been one of the major experimental problems in cuprate superconductivity, particularly when studying dopants or nonstoichiometric systems such as Bi-Sr-Ca-Cu-O. In this paper it is shown that Electron Probe Microanalysis (EPMA) can be used to perform non-destructive stoichiometric analyses of all the elements in single crystals of cuprate superconductors to an accuracy of approximately 2%. The paper gives a detailed description of the special methods that must be employed to obtain this accuracy.

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 Dates: 1991-08-01
 Publication Status: Published in print
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Title: Physica C-Superconductivity and its Applications
  Other : Physica C
Source Genre: Journal
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Publ. Info: Amsterdam : North-Holland
Pages: - Volume / Issue: 178 (4-6) Sequence Number: - Start / End Page: 365 - 376 Identifier: ISSN: 0921-4534
CoNE: /journals/resource/954925564683