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  Flux growth of Sr1−xCaxCuO2 single crystals

Lin, C., Zhou, W., Mackenzie, A. P., Gauthier, F., & Liang, W. (1994). Flux growth of Sr1−xCaxCuO2 single crystals. Journal of Crystal Growth, 140(1-2), 72-78. doi:10.1016/0022-0248(94)90498-7.

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Item Permalink: http://hdl.handle.net/11858/00-001M-0000-0018-E72B-0 Version Permalink: http://hdl.handle.net/11858/00-001M-0000-0018-E731-F
Genre: Journal Article

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 Creators:
Lin, C.T.1, Author
Zhou, W.1, Author
Mackenzie, A. P.2, Author              
Gauthier, F.1, Author
Liang, W.Y.1, Author
Affiliations:
1external, ou_persistent22              
2External Organizations, ou_persistent22              

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 Abstract: A series of single crystals of Sr1-xCaxCuO2, x = 0.19-0.83, has been grown using a low cooling rate in a flux containing excess CuO. Values of the temperature gradient, amount of flux, soaking temperature, soaking time, crucible material and cooling rate have been optimized. The chemical compositions for the as-grown crystals were determined by means of energy dispersive X-ray analysis (EDS) in a transmission electron microscope and confirmed by electron probe microanalysis (EPMA), while the SrCuO2-type structure having orthorhombic symmetry is confirmed by high resolution transmission electron microscopy (HREM). Both the Ca/Sr ratios in the crystals and the unit cell constants vary with a linear relationship with the Ca/Sr ratios in the initial melt.

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 Dates: 1994-06-01
 Publication Status: Published in print
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Title: Journal of Crystal Growth
Source Genre: Journal
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Publ. Info: Amsterdam : North-Holland
Pages: - Volume / Issue: 140 (1-2) Sequence Number: - Start / End Page: 72 - 78 Identifier: ISSN: 0022-0248
CoNE: /journals/resource/954925412860