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  3D strain imaging in sub-micrometer crystals using cross-reciprocal space measurements: Numerical feasibility and experimental methodology

Vaxelaire, N., Labat, S., Chamard, V., Thomas, O., Jacques, V., Picca, F. E., et al. (2010). 3D strain imaging in sub-micrometer crystals using cross-reciprocal space measurements: Numerical feasibility and experimental methodology. Nuclear Instruments and Methods in Physics Research Section B, 268(3-4), 388 -393. doi:10.1016/j.nimb.2009.09.010.

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Genre: Journal Article
Alternative Title : Nuclear Instruments and Methods in Physics Research B

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 Creators:
Vaxelaire, N.1, Author           
Labat, S.1, Author           
Chamard, V.1, Author           
Thomas, O.1, Author           
Jacques, V.2, 3, Author           
Picca, F. E.3, Author           
Ravy, S.3, Author           
Kirchlechner, C.4, 5, Author           
Kečkéš, J.4, 5, Author           
Affiliations:
1Aix-Marseille Université, IM2NP, Campus de Saint-Jérôme, Marseille, France, ou_persistent22              
2Universite Paris-Sud XI, Laboratory of Physics and Solids, Orsay, France, ou_persistent22              
3SOLEIL Synchrotron, Gif-sur-Yvette, France, ou_persistent22              
4Department of Materials Physics, Montanuniversität Leoben, Leoben, Austria, ou_persistent22              
5Erich Schmid Institute of Materials Science, Austrian Academy of Sciences, Leoben, Austria, ou_persistent22              

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 Abstract: Direct inversion of coherent X-ray diffraction patterns is a powerful method to image strains in individual crystals with a high spatial resolution, less than 10 nm. The possibility to invert the diffraction pattern is in principle ensured by the oversampling of the measurement. In addition, the resolution of the reconstructed object requires the measurement of the intensity distribution as far as possible in reciprocal space. Thus, fulfilling the oversampling and resolution constraints, in 3D, implies very long acquisition times, hardly compatible with the stability of the X-ray synchrotron source or sample. To overcome this problem, we present a method based on partial crossed intensity measurements: it consists in two irregularly spaced intensity measurements taken in two orthogonal directions. This paper demonstrates that partial crossed intensity measurements are in principle sufficient to reconstruct 2D objects using a phase retrieval algorithm. We also describe how such measurements can be achieved in practice for 3D imaging. 3D intensity measurements taken in two orthogonal directions for a 111 Bragg peak of a submicrometer Au grain are shown.

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Language(s): eng - English
 Dates: 2010-02
 Publication Status: Issued
 Pages: -
 Publishing info: -
 Table of Contents: -
 Rev. Type: -
 Identifiers: DOI: 10.1016/j.nimb.2009.09.010
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Title: Nuclear Instruments and Methods in Physics Research Section B
  Abbreviation : NIM B
Source Genre: Journal
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Publ. Info: Amsterdam : Elsevier B.V.
Pages: - Volume / Issue: 268 (3-4) Sequence Number: - Start / End Page: 388 - 393 Identifier: ISSN: 0168-583X
CoNE: https://pure.mpg.de/cone/journals/resource/954925484704