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  Mesoscale morphology of airborne core–shell nanoparticle clusters: X-ray laser coherent diffraction imaging

Pedersoli, E., Loh, N. D., Capotondi, F., Hampton, C. Y., Sierra, R. G., Starodub, D., et al. (2013). Mesoscale morphology of airborne core–shell nanoparticle clusters: X-ray laser coherent diffraction imaging. Journal of Physics B, 46(16): 164033, pp. 1-10. doi:10.1088/0953-4075/46/16/164033.

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Item Permalink: http://hdl.handle.net/11858/00-001M-0000-0019-9068-7 Version Permalink: http://hdl.handle.net/11858/00-001M-0000-0019-9069-5
Genre: Journal Article

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 Creators:
Pedersoli, E, Author
Loh, N D, Author
Capotondi, F, Author
Hampton, C Y, Author
Sierra, R G, Author
Starodub, D, Author
Bostedt, C, Author
Bozek, J, Author
Nelson, A J, Author
Aslam, M, Author
Li, S, Author
Dravid, V P, Author
Martin, A V, Author
Aquila, A, Author
Barty, A, Author
Fleckenstein, H, Author
Gumprecht, L, Author
Liang, M, Author
Nass, Karol1, Author              
Schulz, J, Author
White, T A, AuthorCoppola, N, AuthorBajt, S, AuthorBarthelmess, M, AuthorGraafsma, H, AuthorHirsemann, H, AuthorWunderer, C, AuthorEpp, S W, AuthorErk, Benjamin1, Author              Rudek, Benedikt1, Author              Rudenko , A, AuthorFoucar, Lutz1, Author              Kassemeyer, Stefan1, Author              Lomb, Lukas1, Author              Rolles, Daniel1, Author              Shoeman, Robert L.1, Author              Steinbrener, Jan F.1, Author              Hartmann, R, AuthorHartmann, A, AuthorHauser, G, AuthorHoll, P, AuthorKimmel, N, AuthorReich, C, AuthorSoltau, H, AuthorWeidenspointner, G, AuthorBenner, W H, AuthorFarquar, G R, AuthorHau-Riege, S P, AuthorHunter, M S, AuthorEkeberg, T, AuthorHantke, M, AuthorMaia, F R N C, AuthorTobias, H J, AuthorMarchesini, S, AuthorFrank, M, AuthorStrüder, L, AuthorSchlichting, Ilme1, Author              Ullrich, J, AuthorChapman, H N, AuthorBucksbaum, P H, AuthorKiskinova, M, AuthorBogan, M J, Author more..
Affiliations:
1Department of Biomolecular Mechanisms, Max Planck Institute for Medical Research, Max Planck Society, ou_1497700              

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 Abstract: Unraveling the complex morphology of functional materials like core–shell nanoparticles and its evolution in different environments is still a challenge. Only recently has the single-particle coherent diffraction imaging (CDI), enabled by the ultrabright femtosecond free-electron laser pulses, provided breakthroughs in understanding mesoscopic morphology of nanoparticulate matter. Here, we report the first CDI results for Co@SiO2 core–shell nanoparticles randomly clustered in large airborne aggregates, obtained using the x-ray free-electron laser at the Linac Coherent Light Source. Our experimental results compare favourably with simulated diffraction patterns for clustered Co@SiO2 nanoparticles with ~10 nm core diameter and ~30 nm shell outer diameter, which confirms the ability to resolve the mesoscale morphology of complex metastable structures. The findings in this first morphological study of core–shell nanomaterials are a solid base for future time-resolved studies of dynamic phenomena in complex nanoparticulate matter using x-ray lasers.

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Language(s): eng - English
 Dates: 2013-05-232013-03-032013-08-132013-08-28
 Publication Status: Published in print
 Pages: 10
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: DOI: 10.1088/0953-4075/46/16/164033
Other: 7919
 Degree: -

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Title: Journal of Physics B
Source Genre: Journal
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Pages: - Volume / Issue: 46 (16) Sequence Number: 164033 Start / End Page: 1 - 10 Identifier: ISSN: 0953-4075
CoNE: https://pure.mpg.de/cone/journals/resource/954928494403