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  Techniques for analyzing the early stages of crystallization reactions

Schüth, F., Bussian, P., Ågren, P., Schunk, S., & Linden, M. (2001). Techniques for analyzing the early stages of crystallization reactions. Solid State Sciences, 3(7), 801-808. doi:0.1016/S1293-2558(01)01199-2.

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 Creators:
Schüth, Ferdi1, Author              
Bussian, P.1, Author              
Ågren, P.1, Author              
Schunk, S.1, 2, Author              
Linden, M.1, 3, Author              
Affiliations:
1Research Department Schüth, Max-Planck-Institut für Kohlenforschung, Max Planck Society, ou_1445589              
2hteAG, Kurpfalzring 104, 69123 Heidelberg, Germany, ou_persistent22              
3Department of Physical Chemistry, Abo Akademi University, Porthansgatan 3-5, 20500 Abo (Turku), Finland, ou_persistent22              

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Free keywords: Nucleation; Crystallization; Mass spectrometry; Tubular reactor; X-ray diffraction; UV/Vis spectroscopy
 Abstract: This paper will — in a semi-review-like form — describe the problems in analyzing nucleation reactions, and approaches towards a solution of these problems. Attempts to pinpoint the nucleation event can start from the solution state, and the development of precursors for the solid state can be traced with mass spectrometry. Alternatively, one can try to obtain information on ever earlier stages of the solids formation itself, thus approaching the nucleation event from the side of the solid already formed. A highly suitable tool for this purpose is a tubular reactor, where crystallization reactions can be carried out continuously.

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Language(s): eng - English
 Dates: 2001-10-122001
 Publication Status: Published in print
 Pages: -
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: DOI: 0.1016/S1293-2558(01)01199-2
 Degree: -

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Title: Solid State Sciences
Source Genre: Journal
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Publ. Info: Paris : Elsevier Masson SAS
Pages: - Volume / Issue: 3 (7) Sequence Number: - Start / End Page: 801 - 808 Identifier: ISSN: 1293-2558
CoNE: https://pure.mpg.de/cone/journals/resource/954926245540