English
 
Help Privacy Policy Disclaimer
  Advanced SearchBrowse

Item

ITEM ACTIONSEXPORT
  In Situ X-Ray Diffraction Study of the Initial Stages of Formation of MCM-41 in a Tubular Reactor

Linden, M., Schunk, S. A., & Schüth, F. (1998). In Situ X-Ray Diffraction Study of the Initial Stages of Formation of MCM-41 in a Tubular Reactor. Angewandte Chemie International Edition, 37(6), 821-823. doi:10.1002/(SICI)1521-3773(19980403)37:6<821:AID-ANIE821>3.0.CO;2-I.

Item is

Files

show Files

Locators

show

Creators

show
hide
 Creators:
Linden, Mika1, 2, Author              
Schunk, Stephan A.1, Author
Schüth, Ferdi1, Author              
Affiliations:
1Research Department Schüth, Max-Planck-Institut für Kohlenforschung, Max Planck Society, ou_1445589              
2Institut für Anorganische Chemie der Universität, Marie Curie Strasse 11, D-60439 Frankfurt am Main (Germany), ou_persistent22              

Content

show
hide
Free keywords: Mesophases; Mesoporosity; Silicon; X-ray scattering; Zeolite analogues
 Abstract: A continuous process for the synthesis of mesoporous silicates such as MCM-41 at room temperature has been achieved by employing a tubular reactor in which tetraethoxysilane was used as the silicate source (see schematic representation below). The formation of the hexagonal mesophase, which was monitored by using in situ XRD at different points of the tube, was completed in three minutes after mixing of the reactants. The product was stable to calcination, and N2-sorption measurements confirmed the high surface area and narrow pore-size distribution.

Details

show
hide
Language(s): eng - English
 Dates: 1998-12-171998-04-03
 Publication Status: Published in print
 Pages: -
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Degree: -

Event

show

Legal Case

show

Project information

show

Source 1

show
hide
Title: Angewandte Chemie International Edition
  Other : Angew. Chem., Int. Ed.
  Other : Angew. Chem. Int. Ed.
  Other : Angewandte Chemie, International Edition
Source Genre: Journal
 Creator(s):
Affiliations:
Publ. Info: Weinheim : Wiley-VCH
Pages: - Volume / Issue: 37 (6) Sequence Number: - Start / End Page: 821 - 823 Identifier: ISSN: 1433-7851
CoNE: https://pure.mpg.de/cone/journals/resource/1433-7851