English
 
Help Privacy Policy Disclaimer
  Advanced SearchBrowse

Item

ITEM ACTIONSEXPORT
  Synthesis And Sorptive Properties Of Dodecasil 1 H With An Acessible Pore System

Grebner, M., Reichert, H., Schüth, F., & Unger, K. (1994). Synthesis And Sorptive Properties Of Dodecasil 1 H With An Acessible Pore System. In Studies in Surface Science and Catalysis (pp. 545-550). Amsterdam: Elsevier. doi:10.1016/S0167-2991(08)63116-X.

Item is

Files

show Files

Locators

show

Creators

show
hide
 Creators:
Grebner, M.1, Author
Reichert, H.1, Author
Schüth, F.1, 2, Author           
Unger, K.1, Author
Affiliations:
1Institut für Anorganische und Analytische Chemie der Johannes Gutenberg-Universitat Mainz, Becherweg 24, 55099 Mainz, FRG, ou_persistent22              
2Research Department Schüth, Max-Planck-Institut für Kohlenforschung, Max Planck Society, ou_1445589              

Content

show
hide
Free keywords: -
 Abstract: The synthesis of Dodecasil 1H was studied in the system SiO2/1-adamantylamine/NH3/water with the objective of controlling the particle size and the morphology of the crystals. Since nucleation occurs in a very early stage of the synthesis, the heating rate to the final temperature have a strong influence on both parameters. Using seed crystals and such a heating programme, the expensive template 1-adamantylamine can be reduced to so small amounts, that a nearly template free pore system is achieved. The emptiness of the pore system was demonstrated from adsorption measurement using He and H2.

Details

show
hide
Language(s): eng - English
 Dates: 2008-04-141994
 Publication Status: Published in print
 Pages: -
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: DOI: 10.1016/S0167-2991(08)63116-X
 Degree: -

Event

show

Legal Case

show

Project information

show

Source 1

show
hide
Title: Studies in Surface Science and Catalysis
Source Genre: Series
 Creator(s):
Affiliations:
Publ. Info: Amsterdam : Elsevier
Pages: - Volume / Issue: 87 Sequence Number: - Start / End Page: 545 - 550 Identifier: ISSN: 0167-2991
CoNE: https://pure.mpg.de/cone/journals/resource/954926964942_2