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  Simultaneous Determination of the Conformation and Relative Configuration of Archazolide A by Using Nuclear Overhauser Effects, J Couplings, and Residual Dipolar Couplings

Farès, C., Hassfeld, J., Menche, D., & Carlomagno, T. (2008). Simultaneous Determination of the Conformation and Relative Configuration of Archazolide A by Using Nuclear Overhauser Effects, J Couplings, and Residual Dipolar Couplings. Angewandte Chemie International Edition, 47(20), 3722-3726. doi:10.1002/anie.200800225.

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 Creators:
Farès, Christophe1, Author           
Hassfeld, Jorma2, Author
Menche, Dirk3, Author
Carlomagno, Teresa1, Author
Affiliations:
1Department of NMR Based Structural Biology, MPI for Biophysical Chemistry, Max Planck Society, ou_578567              
2Bayer Schering Pharma AG, Müllerstrasse 178, 13342 Berlin, Germany, ou_persistent22              
3Helmholtz‐Zentrum für Infektionsforschung GmbH, Medzinische Chemie, Inhoffenstrasse 7, 38124 Braunschweig, Germany, ou_persistent22              

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Free keywords: conformation analysis; natural products; NMR spectroscopy; polyketides; residual dipolar coupling
 Abstract: Combine and conquer: Configurational assignment of remote stereogenic centers in the complex polyketide macrolide archazolide A (see structure; red O, blue N, yellow S) was accomplished by a purely NMR-based approach relying on a combination of nuclear Overhauser effects, J couplings, and residual dipolar couplings (RDCs).

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Language(s): eng - English
 Dates: 2008-01-162008-04-282008-05-05
 Publication Status: Published in print
 Pages: 5
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: DOI: 10.1002/anie.200800225
 Degree: -

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Title: Angewandte Chemie International Edition
  Abbreviation : Angew. Chem., Int. Ed.
Source Genre: Journal
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Publ. Info: Weinheim : Wiley-VCH
Pages: - Volume / Issue: 47 (20) Sequence Number: - Start / End Page: 3722 - 3726 Identifier: ISSN: 1433-7851
CoNE: https://pure.mpg.de/cone/journals/resource/1433-7851