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  Deciphering ‘water-soluble lignocellulose’ obtained by mechanocatalysis: new insights into the chemical processes leading to deep depolymerization

Käldström, M., Meine, N., Farès, C., Schüth, F., & Rinaldi, R. (2014). Deciphering ‘water-soluble lignocellulose’ obtained by mechanocatalysis: new insights into the chemical processes leading to deep depolymerization. Green Chemistry, 16(7), 3528-3538. doi:10.1039/C4GC00004H.

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 Creators:
Käldström, Mats1, Author              
Meine, Niklas2, Author              
Farès, Christophe3, Author              
Schüth, Ferdi2, Author              
Rinaldi, Roberto1, Author              
Affiliations:
1Research Group Rinaldi, Max-Planck-Institut für Kohlenforschung, Max Planck Society, ou_1445617              
2Research Department Schüth, Max-Planck-Institut für Kohlenforschung, Max Planck Society, ou_1445589              
3Service Department Farès (NMR), Max-Planck-Institut für Kohlenforschung, Max Planck Society, ou_1445623              

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 Abstract: Recently, the mechanocatalytic depolymerization of lignocelluloses yielding ‘water-soluble lignocelluloses’ was demonstrated. Water-soluble C5 & C6 sugars and sulfur-free lignins are formed through the saccharification of the oligosaccharides, allowing for the fractionation of biomass by simple filtration. Herein, we present an in-depth analysis of water-soluble products obtained from beechwood. The complex nature of the ‘water-soluble beechwood’ is investigated by 2D HSQC NMR, HPLC and gel filtration chromatography. The detailed analysis of the ‘water-soluble beechwood’ lends significant insights into the chemical nature of the lignocellulose depolymerization driven by the mechanical forces.

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Language(s): eng - English
 Dates: 2014-01-022014-05-122014-05-122014-07-01
 Publication Status: Published in print
 Pages: 11
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: DOI: 10.1039/C4GC00004H
 Degree: -

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Title: Green Chemistry
  Other : Green Chem.
Source Genre: Journal
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Publ. Info: Cambridge, UK : Royal Society of Chemistry
Pages: - Volume / Issue: 16 (7) Sequence Number: - Start / End Page: 3528 - 3538 Identifier: ISSN: 1463-9262
CoNE: https://pure.mpg.de/cone/journals/resource/954925625301