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  Pyromellitic diimide-porphyrin cyclophanes: Syntheses, transannular interactions and structure analysis

Staab, H. A., Nikolic, S., & Krieger, C. (1999). Pyromellitic diimide-porphyrin cyclophanes: Syntheses, transannular interactions and structure analysis. European Journal of Organic Chemistry, 6, 1459-1470. doi:10.1002/(SICI)1099-0690(199906)1999:6<1459:AID-EJOC1459>3.0.CO;2-7.

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Item Permalink: https://hdl.handle.net/11858/00-001M-0000-0024-AC8B-8 Version Permalink: https://hdl.handle.net/11858/00-001M-0000-0024-AC8C-6
Genre: Journal Article
Alternative Title : Pyromellitic diimide-porphyrin cyclophanes: Syntheses, transannular interactions and structure analysis

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EurJOrgChem_1999_1459.pdf (Any fulltext), 352KB
 
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 Creators:
Staab, Heinz A.1, Author           
Nikolic, Susanne, Author
Krieger, Claus1, Author           
Affiliations:
1Department of Organic Chemistry, Max Planck Institute for Medical Research, Max Planck Society, ou_1497706              

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 Abstract: The acceptor-porphyrin cyclophanes 2 and 4 with pyromellitic diimide (1) as strong electron-acceptor, and the corresponding porphyrin zinc complexes 3 and 5 were prepared by a route which differs considerably from that in the syntheses of previously prepared electron-acceptor porphyrin cyclophanes. The conformations of these electron-acceptor-porphyrin cyclophanes are discussed based on 1H-NMR and the X-ray structural analysis of 2. According to the results obtained, the plane of 1 and that of the porphyrin unit (at least in the crystalline state) are neither close nor parallel to each other. An unusual dihedral orientation of the donor and acceptor planes was detected for 2

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Language(s): eng - English
 Dates: 1998-08-231999
 Publication Status: Issued
 Pages: 12
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: eDoc: 666509
DOI: 10.1002/(SICI)1099-0690(199906)1999:6<1459::AID-EJOC1459>3.0.CO;2-7
URI: http://onlinelibrary.wiley.com/doi/10.1002/(SICI)1099-0690(199906)1999:6%3C1459::AID-EJOC1459%3E3.0.CO;2-7/abstract
Other: 4474
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Title: European Journal of Organic Chemistry
  Other : Eur. J. Org. Chem.
Source Genre: Journal
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Publ. Info: Weinheim, Germany : Wiley-VCH
Pages: - Volume / Issue: 6 Sequence Number: - Start / End Page: 1459 - 1470 Identifier: ISSN: 1434-193X
CoNE: https://pure.mpg.de/cone/journals/resource/954926953810