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  Crystal structure redetermination of the D,L-glyceraldehyde dimer: A comparison of synchrotron and conventional X-ray diffraction data

Lehmann, C. W., & Luger, P. (1991). Crystal structure redetermination of the D,L-glyceraldehyde dimer: A comparison of synchrotron and conventional X-ray diffraction data. Zeitschrift für Kristallographie-Crystalline Materials, 195(1-2), 49-63. doi:10.1524/zkri.1991.195.1-2.49.

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Item Permalink: https://hdl.handle.net/11858/00-001M-0000-0024-C263-C Version Permalink: https://hdl.handle.net/21.11116/0000-0007-0F09-0
Genre: Journal Article

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 Creators:
Lehmann, Christian W.1, Author           
Luger, Peter1, Author
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1Institut für Kristallographie, Freie Universität Berlin, Takustr. 6, D-1000 Berlin 33, West Germany, ou_persistent22              

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 Abstract: The structure of D,L-glyceraldehyde has been redetermined by means of synchrotron and conventional X-radiation. At 295 K lattice parameters in monoclinic space group P21/n are: a=6.403(2)Å, b= 6.961(2)Å, c=8.830(3)Å, beta=105.00(2)°, V=380.12Å3, Z=2. Three independent data sets of crystals with
crystal volumes of 0.00009 and 0.02mm3 are compared. As a main advantage of the synchrotron experiment it was found that its results obtained with the small crystal are of similar precision compared to those based on the larger crystal measured with a conventional tube.

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Language(s): eng - English
 Dates: 1991-01
 Publication Status: Issued
 Pages: 15
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: DOI: 10.1524/zkri.1991.195.1-2.49
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Title: Zeitschrift für Kristallographie-Crystalline Materials
  Abbreviation : Z. Kristallogr. - Cryst. Mater.
Source Genre: Journal
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Publ. Info: Berlin/Boston : de Gruyter
Pages: - Volume / Issue: 195 (1-2) Sequence Number: - Start / End Page: 49 - 63 Identifier: ISSN: 2194-4946
CoNE: https://pure.mpg.de/cone/journals/resource/2194-4946