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  Direct Imaging of Octahedral Distortion in a Complex Molybdenum Vanadium Mixed Oxide

Lunkenbein, T., Girgsdies, F., Wernbacher, A. M., Noack, J., Auffermann, G., Yasuhara, A., et al. (2015). Direct Imaging of Octahedral Distortion in a Complex Molybdenum Vanadium Mixed Oxide. Angewandte Chemie, 127(23), 6932-6935. doi:10.1002/ange.201502236.

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 Creators:
Lunkenbein, Thomas1, Author           
Girgsdies, Frank1, Author           
Wernbacher, Anna Maria1, Author           
Noack, Johannes1, Author           
Auffermann, G.2, Author           
Yasuhara, Akira3, Author
Klein-Hoffmann, Achim1, Author           
Ueda, Wataru4, Author
Eichelbaum, Maik1, Author           
Trunschke, Annette1, Author           
Schlögl, Robert1, 5, Author           
Willinger, Marc Georg1, Author           
Affiliations:
1Inorganic Chemistry, Fritz Haber Institute, Max Planck Society, ou_24023              
2Gudrun Auffermann, Inorganic Chemistry, Max Planck Institute for Chemical Physics of Solids, Max Planck Society, ou_1863432              
3Jeol Ltd., Tokyo (Japan), ou_persistent22              
4Catalysis Research Center, Hokkaido University, Sapporo (Japan), ou_persistent22              
5Max-Planck-Institut für Chemische Energiekonversion, Stiftstrasse 34–36, 45470 Mülheim an der Ruhr, Germany, ou_persistent22              

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Free keywords: Aberrationskorrigierte Elektronenmikroskopie; Bindungswinkel; Hell- und Dunkelfeldmikroskopie; Leichte Elemente; Transmissionselektronenmikroskopie
 Abstract: Complex Mo,V-based mixed oxides that crystallize in the orthorhombic M1-type structure are promising candidates for the selective oxidation of small alkanes. The oxygen sublattice of such a complex oxide has been studied by annular bright field scanning transmission electron microscopy. The recorded micrographs directly display the local distortion in the metal oxygen octahedra. From the degree of distortion we are able to draw conclusions on the distribution of oxidation states in the cation columns at different sites. The results are supported by X-ray diffraction and electron paramagnetic resonance measurements that provide integral details about the crystal structure and spin coupling, respectively.

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Language(s): eng - English
 Dates: 2015-03-102015-04-272015-06-01
 Publication Status: Published in print
 Pages: 4
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: DOI: 10.1002/ange.201502236
 Degree: -

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Title: Angewandte Chemie
  Abbreviation : Angew. Chem.
Source Genre: Journal
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Publ. Info: Weinheim : Wiley-VCH
Pages: - Volume / Issue: 127 (23) Sequence Number: - Start / End Page: 6932 - 6935 Identifier: ISSN: 0044-8249
CoNE: https://pure.mpg.de/cone/journals/resource/954926979058_1