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  Application of Ambient-Pressure X-ray Photoelectron Spectroscopy for the In-situ Investigation of Heterogeneous Catalytic Reactions

Starr, D. E., Bluhm, H., Liu, Z., Knop-Gericke, A., & Hävecker, M. (2013). Application of Ambient-Pressure X-ray Photoelectron Spectroscopy for the In-situ Investigation of Heterogeneous Catalytic Reactions. In J. A. Rodriguez, J. C. Hanson, & P. J. Chupas (Eds.), In-situ Characterization of Heterogeneous Catalysts (pp. 315-343). Weinheim: Wiley-VCH. doi:10.1002/9781118355923.ch12.

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Item Permalink: https://hdl.handle.net/11858/00-001M-0000-0027-D2D8-F Version Permalink: https://hdl.handle.net/11858/00-001M-0000-0029-2FA1-8
Genre: Book Chapter

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In situ XPS for Chem Soc Rev_revised_DES_HB.pdf (Any fulltext), 2MB
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2015
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Wiley-VCH
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 Creators:
Starr, David E.1, Author
Bluhm, Hendrik2, Author
Liu, Zhi3, Author
Knop-Gericke, Axel4, Author           
Hävecker, Michael5, Author
Affiliations:
1Center for Functional Nanomaterials, Brookhaven National Laboratory, Upton, NY, ou_persistent22              
2Chemical Seiences Division, Lawrence Berkeley National Laboratory, Berkeley, CA, ou_persistent22              
3Advanced Light Source, Lawrence Berkeley National Laboratory, Berkeley, CA, ou_persistent22              
4Inorganic Chemistry, Fritz Haber Institute, Max Planck Society, ou_24023              
5Division Solar Energy Research, Elektronenspeicherring BESSY II,, Berlin, Germany, ou_persistent22              

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Free keywords: ambient-pressure X-ray photoelectron spectroscopy (AP-XPS); carbon nanotubes (CNTs); crystal substrates; electrochemistry; heterogeneous catalytic reactions; carbon nanotube growth; preferential co oxidation; mixed-oxide catalysts; propane oxidation; hydrogen prox; m1 phase; surface; water; nanoparticles; liquids
 Abstract: The desire to carry out X-ray photoelectron spectroscopy (XPS) measurements at elevated pressure conditions has existed for decades and numerous research groups have contributed to the development of a modern form of XPS that can be used at gas pressures up to about 7 mbar. This technique is currently known as ambient-pressure (AP) XPS. This chapter provides an overview of the historical development of AP-XPS addressing specific technical advances and their relevance. It provides examples of the application of AP-XPS. These examples demonstrate the versatility of this technique for the investigation of catalytically relevant systems ranging from structurally well-defined systems composed of adsorbates on single crystal surfaces and nanoparticles, the catalytic growth of nanotubes, to operating electrochemical cells and industrial heterogeneous catalysts.

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Language(s): eng - English
 Dates: 2013-06-282013-06-10
 Publication Status: Issued
 Pages: -
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: ISBN: 978-1-118-00016-8
ISBN: 978-1-118-35592-3
DOI: 10.1002/9781118355923.ch12
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Title: In-situ Characterization of Heterogeneous Catalysts
Source Genre: Book
 Creator(s):
Rodriguez, José A, Editor
Hanson, Jonathan C, Editor
Chupas, Peter J, Editor
Affiliations:
-
Publ. Info: Weinheim : Wiley-VCH
Pages: - Volume / Issue: - Sequence Number: - Start / End Page: 315 - 343 Identifier: -