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  Synthesis of Supported Ga Nanodrops by a Bottom-up Route

Armbrüster, M., & Cardoso-Gil, R. (2015). Synthesis of Supported Ga Nanodrops by a Bottom-up Route. Zeitschrift für anorganische und allgemeine Chemie, 641(8-9), 1453-1458. doi:10.1002/zaac.201500155.

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Item Permalink: http://hdl.handle.net/11858/00-001M-0000-0028-5068-5 Version Permalink: http://hdl.handle.net/21.11116/0000-0000-FFF7-B
Genre: Journal Article

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 Creators:
Armbrüster, Marc1, Author
Cardoso-Gil, Raul2, Author              
Affiliations:
1External Organizations, ou_persistent22              
2Raul Cardoso, Chemical Metal Science, Max Planck Institute for Chemical Physics of Solids, Max Planck Society, ou_1863420              

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 Abstract: Nanoparticulate gallium can be obtained in an unconfined state by reduction of gallium-acetylacetonate with LiAlH4. The products were analyzed by scanning electron microscopy, elemental analysis together with X-ray diffraction, and thermal analysis. EXAFS investigations reveal, in accordance with the results from thermal analyses, that the particles are liquid at room temperature. The reason for the lower melting point could not be clarified within this study and might be caused either by the lower melting point of -gallium or by the small particle size of 10-20 nm. Upon cooling, several of the low-temperature modifications of gallium are observed depending on cooling-rate and temperature.

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Language(s): eng - English
 Dates: 2015-05-072015-05-07
 Publication Status: Published in print
 Pages: -
 Publishing info: -
 Table of Contents: -
 Rev. Method: -
 Identifiers: ISI: 000358134700009
DOI: 10.1002/zaac.201500155
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Title: Zeitschrift für anorganische und allgemeine Chemie
  Other : Journal of Inorganic and General Chemistry
  Other : J. Inorg. Gen Chem.
  Abbreviation : Z. Anorg. Allg. Chem.
Source Genre: Journal
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Publ. Info: Weinheim : Wiley-VCH
Pages: - Volume / Issue: 641 (8-9) Sequence Number: - Start / End Page: 1453 - 1458 Identifier: ISSN: 0044-2313
CoNE: https://pure.mpg.de/cone/journals/resource/954925453895