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  Access to side-chain carbon information in deuterated solids under fast MAS through non-rotor-synchronized mixing.

Kulminskaya, N., Vasa, S. K., Giller, K., Becker, S., Kwan, A., Sunde, M., et al. (2016). Access to side-chain carbon information in deuterated solids under fast MAS through non-rotor-synchronized mixing. Chemical Communications, 52(2), 268-271. doi:10.1039/C5CC07345F.

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Item Permalink: http://hdl.handle.net/11858/00-001M-0000-0028-EA2C-3 Version Permalink: http://hdl.handle.net/11858/00-001M-0000-002C-D112-E
Genre: Journal Article

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 Creators:
Kulminskaya, N.1, Author              
Vasa, S. K.2, Author              
Giller, K.1, Author              
Becker, S.1, Author              
Kwan, A., Author
Sunde, M., Author
Linser, R.2, Author              
Affiliations:
1Department of NMR-Based Structural Biology, MPI for biophysical chemistry, Max Planck Society, ou_578567              
2Research Group of Solid-State NMR-2, MPI for Biophysical Chemistry, Max Planck Society, ou_1950286              

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 Abstract: We demonstrate the accessibility of aliphatic 13C side chain chemical shift sets for solid-state NMR despite perdeuteration and fast MAS using isotropic, non-rotor-synchronized 13C-13C mixing. Combined with amide proton detection, we unambiguously and sensitively detect whole side chain to backbone correlations for two proteins using around 1 mg of sample.

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Language(s): eng - English
 Dates: 2015-10-222016-01-07
 Publication Status: Published in print
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 Rev. Method: Peer
 Identifiers: DOI: 10.1039/C5CC07345F
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Title: Chemical Communications
Source Genre: Journal
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Pages: - Volume / Issue: 52 (2) Sequence Number: - Start / End Page: 268 - 271 Identifier: -