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  Phase transition kinetics and reorientational dynamics of the plastic crystal meta-carborane studied by deuteron NMR

Winterlich, M., Zimmermann, H., & Böhmer, R. (2002). Phase transition kinetics and reorientational dynamics of the plastic crystal meta-carborane studied by deuteron NMR. Journal of Non-Crystalline Solids, 307-310, 442-448. doi:10.1016/S0022-3093(02)01506-5.

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Item Permalink: https://hdl.handle.net/11858/00-001M-0000-0029-7D6D-B Version Permalink: https://hdl.handle.net/11858/00-001M-0000-0029-7D6E-9
Genre: Journal Article
Alternative Title : Phase transition kinetics and reorientational dynamics of the plastic crystal meta-carborane studied by deuteron NMR

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JNonCrystalSolids_307_2002_442.pdf (Any fulltext), 205KB
 
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 Creators:
Winterlich, Manfred, Author
Zimmermann, Herbert1, Author           
Böhmer, Roland, Author
Affiliations:
1Emeritus Group Biophysics, Max Planck Institute for Medical Research, Max Planck Society, ou_1497712              

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Free keywords: O150; N220; P130PACS classification codes: 64.60.Cn; 64.60.My; 76.60.-K; 64.70.Pf
 Abstract: Meta-carborane shows an orientationally disordered, orthorhombic phase which transforms into an ordered monoclinic phase near 170 K and into a quasi-isotropic cubic phase near 280 K. From deuteron magnetization measurements both transitions are found to exhibit a thermal hysteresis and slow transformation kinetics. Furthermore, solid-echo NMR spectra and spin-lattice relaxation times are reported. These results indicate that in the orthorhombic phase the meta-carborane molecules perform a strongly anisotropic motion which is characterized by a temperature dependent amplitude.

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Language(s): eng - English
 Dates: 2002-06-042002-09
 Publication Status: Issued
 Pages: 7
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: eDoc: 666138
DOI: 10.1016/S0022-3093(02)01506-5
URI: http://www.sciencedirect.com/science/article/pii/S0022309302015065
Other: 5287
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Title: Journal of Non-Crystalline Solids
Source Genre: Journal
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Publ. Info: Amsterdam : North-Holland
Pages: - Volume / Issue: 307-310 Sequence Number: - Start / End Page: 442 - 448 Identifier: ISSN: 0022-3093
CoNE: https://pure.mpg.de/cone/journals/resource/954925416961