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  A combined 17O RAPT and MQ-MAS NMR study of L-leucine

Prasad, S., Clark, T. M., Sharma, R., Kwak, H.-T., Grandinetti, P. J., & Zimmermann, H. (2006). A combined 17O RAPT and MQ-MAS NMR study of L-leucine. Solid State Nuclear Magnetic Resonance, 29(1-3), 119-124. doi:10.1016/j.ssnmr.2005.10.007.

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Item Permalink: https://hdl.handle.net/11858/00-001M-0000-002A-EE2B-B Version Permalink: https://hdl.handle.net/11858/00-001M-0000-002A-EE2C-9
Genre: Journal Article
Alternative Title : A combined 17O RAPT and MQ-MAS NMR study of L-leucine

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SolidStateNMR_29_2006_119.pdf (Any fulltext), 208KB
 
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 Creators:
Prasad, Subramanian, Author
Clark, Ted M., Author
Sharma, Ramesh, Author
Kwak, Hyung-Tae, Author
Grandinetti, Philip J., Author
Zimmermann, Herbert1, Author           
Affiliations:
1Department of Biomolecular Mechanisms, Max Planck Institute for Medical Research, Max Planck Society, ou_1497700              

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Free keywords: Amino acids; RAPT; MQ-MAS
 Abstract: We report the application of rotor-assisted population transfer (RAPT) to measure the quadrupolar coupling constant (C(q)) for spin 5/2 nuclei. Results from numerical simulations are presented on the magnitude of enhancement factor as a function of frequency offsets, i.e. the RAPT profile. Experimental O17 RAPT profile is traced for the amino acid L-leucine. In addition, results from MQ-MAS experiments are incorporated to determine the quadrupolar asymmetry parameter (eta(q)). Unlike previous reports, the O17 NMR parameters for an amino acid, L-leucine, is reported at a relatively low field of 9.4 T.

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Language(s): eng - English
 Dates: 2005-10-042005-06-282005-11-152005-11-152006-02-01
 Publication Status: Issued
 Pages: 6
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Identifiers: eDoc: 665488
DOI: 10.1016/j.ssnmr.2005.10.007
URI: http://www.ncbi.nlm.nih.gov/pubmed/16293400
URI: http://www.sciencedirect.com/science/article/pii/S0926204005000986
Other: 6514
 Degree: -

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Title: Solid State Nuclear Magnetic Resonance
Source Genre: Journal
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Publ. Info: San Diego, CA : Academic Press
Pages: - Volume / Issue: 29 (1-3) Sequence Number: - Start / End Page: 119 - 124 Identifier: ISSN: 0926-2040
CoNE: https://pure.mpg.de/cone/journals/resource/954925567752