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  Lipopolysaccharide core region of Hafnia alvei: structure elucidation using chemical methods, gas chromatography-mass spectrometry, and NMR spectroscopy

Gamian, A., Katzenellenbogen, E., Romanowska, E., Dabrowski, U., & Dabrowski, J. (1995). Lipopolysaccharide core region of Hafnia alvei: structure elucidation using chemical methods, gas chromatography-mass spectrometry, and NMR spectroscopy. Carbohydrate Research, 266(2), 221-228. doi:10.1016/0008-6215(94)00266-I.

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CarbohydRes_266_1995_221.pdf (Any fulltext), 628KB
 
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 Creators:
Gamian, Andrzej, Author
Katzenellenbogen, Ewa, Author
Romanowska, Elzbieta, Author
Dabrowski, Ursula1, Author              
Dabrowski, Janusz1, Author              
Affiliations:
1Department of Organic Chemistry, Max Planck Institute for Medical Research, Max Planck Society, ou_1497706              

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Free keywords: Lipopolysaccharide; Core oligosaccharide; Hafnia alvei; NMR
 Abstract: Sugar and methylation analysis with the use of gas chromatography+mass spectrometry and lit NMR spectroscopy proved that the core oligosaccharides isolated from lipopolysaccharides of eight Hajhia alvei strains have the identical hexasaccharide skeleton. However, tH,3tP heterocorrelatcd spectra showed that the phosphorylation pattern is not the same. The branched heptose for the ATCC 13337, 1187, 2, 1191, 1196, 1220, and 481L strains is pbosphorylated as in the following formula, where P =-O-P(O) (O-)2 and P-PEtN=[-O-P(O) (O-)]2-O(CH2) 2NH+3 α-LD-Hepp 1 ↓ 7 α-D-Glcp-(1 → 3) -α-D-Glcp-(1 →3)-α-LD-Hepp-(1 → 3)- α-LD-Hepp- ( 1 → 5 )-Kdo |4|4 P P-P-EtN

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Language(s): eng - English
 Dates: 1994-04-051994-08-021995-01-17
 Publication Status: Published in print
 Pages: 8
 Publishing info: -
 Table of Contents: -
 Rev. Type: Peer
 Degree: -

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Title: Carbohydrate Research
  Other : Carbohydrate Research
Source Genre: Journal
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Publ. Info: Amsterdam : Elsevier
Pages: - Volume / Issue: 266 (2) Sequence Number: - Start / End Page: 221 - 228 Identifier: ISSN: 0008-6215
CoNE: https://pure.mpg.de/cone/journals/resource/954925388219