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  Continuous synthesis of nanostructured silica based materials in a gas–liquid segmented flow tubular reactor

Knossalla, J., Mezzavilla, S., & Schüth, F. (2016). Continuous synthesis of nanostructured silica based materials in a gas–liquid segmented flow tubular reactor. New Journal of Chemistry, 40(5), 4361-4366. doi:10.1039/C5NJ03033A.

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 Creators:
Knossalla, Johannes1, Author              
Mezzavilla, Stefano2, Author              
Schüth, Ferdi2, Author              
Affiliations:
1Department of Heterogeneous Catalysis, Max-Planck-Institut für Kohlenforschung, Kaiser-Wilhelm-Platz 1, 45470 Mülheim an der Ruhr, Germany, ou_persistent22              
2Research Department Schüth, Max-Planck-Institut für Kohlenforschung, Max Planck Society, ou_1445589              

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 Abstract: A continuous synthesis of several spherical silica structures – by means of a gas–liquid segmented flow tubular reactor – is reported. Specifically, as proof of concept, we showed that 300–400 nm mesoporous core–shell spheres (SiO2@mSiO2), mesoporous spheres (mSiO2) as well gold-encapsulated spheres (Au@SiO2) can be effectively produced in a continuous manner in a tubular reactor. Thus, the successful conversion of classical batch methods to continuous processes opens new possibilities for the up-scaled synthesis of advanced nanostructured materials.

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Language(s): eng - English
 Dates: 2016-03-152016-05-01
 Publication Status: Published in print
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 Table of Contents: -
 Rev. Type: Peer
 Identifiers: DOI: 10.1039/C5NJ03033A
 Degree: -

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Title: New Journal of Chemistry
  Other : NJoC
Source Genre: Journal
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Publ. Info: Paris : CNRS/Gauthier-Villars
Pages: - Volume / Issue: 40 (5) Sequence Number: - Start / End Page: 4361 - 4366 Identifier: ISSN: 1144-0546
CoNE: https://pure.mpg.de/cone/journals/resource/954928578776