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  Robust refocusing of 13C magnetization in multidimensional NMR experiments by adiabatic fast passage pulses.

Zweckstetter, M., & Holak, T. A. (1999). Robust refocusing of 13C magnetization in multidimensional NMR experiments by adiabatic fast passage pulses. Journal of Biomolecular NMR, 15(4), 331-334. doi:10.1023/A:1008360013567.

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Item Permalink: http://hdl.handle.net/11858/00-001M-0000-002B-A56D-A Version Permalink: http://hdl.handle.net/11858/00-001M-0000-002B-A570-D
Genre: Journal Article

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2353722.pdf (Publisher version), 68KB
 
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 Creators:
Zweckstetter, M.1, Author              
Holak, T. A., Author
Affiliations:
1Research Group of Protein Structure Determination using NMR, MPI for biophysical chemistry, Max Planck Society, ou_578571              

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 Abstract: We show that adiabatic fast passage (AFP) pulses are robust refocusing elements of transverse 13C magnetization in multidimensional NMR experiments. A pair of identical AFP pulses can refocus selected parts or a complete 13 C chemical shift range in 13C spectra. In the constant time 13C-1H HSQC, replacement of attenuated rectangular pulses by selective AFP pulses results in a sensitivity enhancement of up to a factor of 1.8. In the 3D CBCA(CO)NH the signal-to-noise ratio is increased by a factor of up to 1.6.

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Language(s): eng - English
 Dates: 1999-12
 Publication Status: Published in print
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 Rev. Method: Peer
 Identifiers: DOI: 10.1023/A:1008360013567
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Title: Journal of Biomolecular NMR
Source Genre: Journal
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Pages: - Volume / Issue: 15 (4) Sequence Number: - Start / End Page: 331 - 334 Identifier: -