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  Electrochemical synthesis and crystal structure of zinc(II) complexes with N2N′2S2 amide–thioether hexadentate ligands.

Meghdadi, S., Mirkhani, V., Kia, R., Moghadam, M., Tangestaninejad, S., & Mohammadpoor-Baltork, I. (2012). Electrochemical synthesis and crystal structure of zinc(II) complexes with N2N′2S2 amide–thioether hexadentate ligands. Polyhedron, 41(1), 115-119. doi:10.1016/j.poly.2012.04.032.

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Item Permalink: http://hdl.handle.net/11858/00-001M-0000-002C-0C42-B Version Permalink: http://hdl.handle.net/11858/00-001M-0000-002C-0C45-5
Genre: Journal Article

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2367049.pdf (Publisher version), 464KB
 
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 Creators:
Meghdadi, S., Author
Mirkhani, V., Author
Kia, R.1, Author              
Moghadam, M., Author
Tangestaninejad, S., Author
Mohammadpoor-Baltork, I., Author
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1Research Group of Structural Dynamics of (Bio)Chemical Systems, MPI for Biophysical Chemistry, Max Planck Society, ou_578564              

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 Abstract: Three novel complexes of zinc with hexadentate amide–thioether ligands were synthesized by electrochemical oxidation of zinc in dichloromethane–methanol solution. These compounds were characterized by elemental analyses, 1H NMR, and IR spectroscopy. The molecular structures of two complexes were determined by single crystal X-ray diffraction, indicating that, the metal atom is in a distorted octahedral environment with amide–thioether ligand acting as a hexadentate N2N′2S2 donor.

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Language(s): eng - English
 Dates: 2012-05-052012-06-28
 Publication Status: Published in print
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 Rev. Method: Peer
 Identifiers: DOI: 10.1016/j.poly.2012.04.032
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Title: Polyhedron
Source Genre: Journal
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Pages: - Volume / Issue: 41 (1) Sequence Number: - Start / End Page: 115 - 119 Identifier: -