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  An endstation for resonant inelastic X-ray scattering studies of solid and liquid samples.

Yin, Z., Peters, H. B., Hahn, U., Gonschior, J., Mierwaldt, D., Rajkovic, I., et al. (2017). An endstation for resonant inelastic X-ray scattering studies of solid and liquid samples. Journal of Synchrotron Radiation, 24(1), 302-306. doi:10.1107/S1600577516016611.

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Item Permalink: http://hdl.handle.net/11858/00-001M-0000-002C-0C9E-0 Version Permalink: http://hdl.handle.net/21.11116/0000-0001-57C6-E
Genre: Journal Article

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2367089.pdf (Publisher version), 736KB
 
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 Creators:
Yin, Z.1, Author              
Peters, H. B., Author
Hahn, U., Author
Gonschior, J., Author
Mierwaldt, D., Author
Rajkovic, I.1, Author              
Viefhaus, J., Author
Jooss, C., Author
Techert, S.1, Author              
Affiliations:
1Research Group of Structural Dynamics of (Bio)Chemical Systems, MPI for biophysical chemistry, Max Planck Society, ou_578564              

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Free keywords: RIXS; Varied line spacing; Liquid jet; XAS; XES; FEL
 Abstract: A novel experimental setup is presented for resonant inelastic X-ray scattering investigations of solid and liquid samples in the soft X-ray region for studying the complex electronic configuration of (bio)chemical systems. The uniqueness of the apparatus is its high flexibility combined with optimal energy resolution and energy range ratio. The apparatus enables investigation of chemical analyses, which reflects the chemical imprints. The endstation is composed of a main sample chamber, a sample holder for either solid or liquid jet delivery system, and a soft X-ray grating spectrometer for 210–1250 eV with a resolving power of 1000. It combines for the first time liquid jet technology with a soft X-ray spectrometer based on the variable line spacing principle. This setup was commissioned at the soft X-ray beamline P04 at PETRA III of the Deutsches Elektronen-Synchrotron in Hamburg which is currently the most brilliant storage-ring-based X-ray radiation source in the world. The first results of liquid and solid samples show that this setup allows the detection of photons across an energy range of 300 eV. This covers simultaneously the emission lines of life- important elements like carbon, nitrogen and oxygen in a shot-based procedure.

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Language(s): eng - English
 Dates: 2017-01-01
 Publication Status: Published online
 Pages: -
 Publishing info: -
 Table of Contents: -
 Rev. Method: Peer
 Identifiers: DOI: 10.1107/S1600577516016611
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Title: Journal of Synchrotron Radiation
Source Genre: Journal
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Pages: - Volume / Issue: 24 (1) Sequence Number: - Start / End Page: 302 - 306 Identifier: -