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  Efficient, solvent-free hydrogenation of α-angelica lactone catalysed by Ru/C at atmospheric pressure and room temperature

Al Shaal, M. G., Hausoul, P. J. C., & Palkovits, R. (2014). Efficient, solvent-free hydrogenation of α-angelica lactone catalysed by Ru/C at atmospheric pressure and room temperature. Chemical Communications, 50(71), 10206-10209. doi:10.1039/C4CC03970J.

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Item Permalink: https://hdl.handle.net/11858/00-001M-0000-002C-8648-3 Version Permalink: https://hdl.handle.net/11858/00-001M-0000-002C-8649-1
Genre: Journal Article

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 Creators:
Al Shaal, Mohammad Ghith1, Author           
Hausoul, Peter J. C.2, Author
Palkovits, Regina2, 3, Author           
Affiliations:
1Research Department Schüth, Max-Planck-Institut für Kohlenforschung, Max Planck Society, ou_1445589              
2Institut für Technische und Makromolekulare Chemie, RWTH Aachen University, Worringerweg 1, Aachen, Germany , ou_persistent22              
3Research Group Palkovits, Max-Planck-Institut für Kohlenforschung, Max Planck Society, ou_1445615              

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 Abstract: The hydrogenation of α-angelica lactone was investigated over Ru/C. A mild protocol was developed, which resulted in full conversion and 96% selectivity toward γ-valerolactone. The reaction network was investigated and α-angelica lactone was employed in the one-pot conversion into 2-methyltetrahydrofuran, demonstrating its superiority as a platform molecule in potential biorefinery schemes.

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Language(s): eng - English
 Dates: 2014-07-162014-09-14
 Publication Status: Issued
 Pages: -
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 Table of Contents: -
 Rev. Type: Peer
 Identifiers: DOI: 10.1039/C4CC03970J
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Title: Chemical Communications
  Other : Chem. Commun.
Source Genre: Journal
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Publ. Info: Cambridge, UK : Royal Society of Chemistry
Pages: - Volume / Issue: 50 (71) Sequence Number: - Start / End Page: 10206 - 10209 Identifier: ISSN: 1359-7345
CoNE: https://pure.mpg.de/cone/journals/resource/954928495413