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  Electron spin resonance of fluorine-substituted nitro-aromatic anion radicals

Fischer, P. H. H., & Zimmermann, H. (1968). Electron spin resonance of fluorine-substituted nitro-aromatic anion radicals. Canadian Journal of Chemistry, 46(24), 3847-3856. doi:10.1139/v68-638.

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CanJChem_46_1968_3847.pdf (Any fulltext), 492KB
 
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 Creators:
Fischer, Peter H. H.1, Author           
Zimmermann, Herbert2, Author           
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1Max Planck Institute for Medical Research, Max Planck Society, ou_1125545              
2Department of Biomolecular Mechanisms, Max Planck Institute for Medical Research, Max Planck Society, ou_1497700              

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 Abstract: Electron spin resonance spectra have been observed for anion radicals derived from 2-fluoro-nitro-benzene, 3-fluoro-nitrobenzene, 2,4-difluoro-nitrobenzene, 2,5-difluoro-nitrobenzene, 4-fluoro-2-nitro-phenol, 2-fluoro-6-nitrophenol, and 3-fluoro-6-nitrophenol. All radicals were generated electrolytically in dimethoxyethane/acetonitrile solution, acetonitrile, or dimethylformamide. The radicals are generally quite stable with the exception of those from 2-fluoro-6-nitrophenol and 3-fluoro-6-nitrophenol, the latter decaying with a half-life of approximately 6 min. All spectra can be interpreted completely, and coupling constants are assigned by comparison to related compounds and consistency arguments.

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Language(s): eng - English
 Dates: 1968-05-131968
 Publication Status: Published in print
 Pages: 10
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 Rev. Type: Peer
 Identifiers: DOI: 10.1139/v68-638
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Title: Canadian Journal of Chemistry
Source Genre: Journal
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Publ. Info: Ottawa, Canada : NRC Research Press
Pages: - Volume / Issue: 46 (24) Sequence Number: - Start / End Page: 3847 - 3856 Identifier: ISSN: 0008-4042
CoNE: https://pure.mpg.de/cone/journals/resource/954925388196_1