A new type of multiplet effect in dynamic nuclear polarization of 13C-nuclei

Buchner, W.; Emmerich, B.

doi:10.1016/0022-2364(71)90028-X

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A new type of multiplet effect in dynamic nuclear polarization of 13C-nuclei

Buchner, W., & Emmerich, B. (1971). A new type of multiplet effect in dynamic nuclear polarization of 13C-nuclei. Journal of Magnetic Resonance, 4(1), 90-98. doi:10.1016/0022-2364(71)90028-X.

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Buchner, W.¹, Author
Emmerich, B.¹, Author

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1Max Planck Institute for Medical Research, Max Planck Society, ou_1125545

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Abstract: The inner lines of the 13C NMR quartet of a free radical solution in α-13C-toluene have been observed to be more negatively enhanced in a DNP experiment than the outer ones, which are, in fact, even positively enhanced at low free radical concentration. The results are interpreted in terms of the three-spin effect. The unusual appearance of the DNP-enhanced 13C quartet originates from the dipolar relaxation within a methyl group undergoing nearly free rotation.

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Language(s): eng - English

Dates: Submitted: 1970-07-28Accepted: 1970-09-14Published Online: 2004-06-29Date issued: 1971-02

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Pages: 9

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Identifiers: DOI: 10.1016/0022-2364(71)90028-X

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Title: Journal of Magnetic Resonance

Source Genre: Journal

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Publ. Info: San Diego [etc.] : Academic Press

Pages: - Volume / Issue: 4 (1) Sequence Number: - Start / End Page: 90 - 98 Identifier: ISSN: 0022-2364
CoNE: https://pure.mpg.de/cone/journals/resource/954922651175_1