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  1,3-Dibromo-5,5-dimethylhydantoin as promoter for glycosylations using thioglycosides

Xu, F.-F., Pereira, C. L., & Seeberger, P. H. (2017). 1,3-Dibromo-5,5-dimethylhydantoin as promoter for glycosylations using thioglycosides. Beilstein Journal of Organic Chemistry, 13, 1994-1998. doi:10.3762/bjoc.13.195.

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Item Permalink: http://hdl.handle.net/11858/00-001M-0000-002D-FD44-0 Version Permalink: http://hdl.handle.net/21.11116/0000-0006-5E37-4
Genre: Journal Article

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 Creators:
Xu, Fei-Fei1, Author              
Pereira, Claney L.1, Author              
Seeberger, Peter H.1, Author              
Affiliations:
1Peter H. Seeberger - Vaccine Development, Biomolekulare Systeme, Max Planck Institute of Colloids and Interfaces, Max Planck Society, ou_1863308              

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Free keywords: Open Access
 Abstract: 1,3-Dibromo-5,5-dimethylhydantoin (DBDMH), an inexpensive, non-toxic and stable reagent, is a competent activator of thioglycosides for glycosidic bond formation. Excellent yields were obtained when triflic acid (TfOH) or trimethylsilyl trifluoromethanesulfonate (TMSOTf) were employed as co-promoters in solution or automated glycan assembly on solid phase.

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 Dates: 2017
 Publication Status: Published in print
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 Rev. Type: -
 Identifiers: DOI: 10.3762/bjoc.13.195
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Title: Beilstein Journal of Organic Chemistry
Source Genre: Journal
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Publ. Info: Frankfurt, Germany : Beilstein-Institut
Pages: - Volume / Issue: 13 Sequence Number: - Start / End Page: 1994 - 1998 Identifier: ISSN: 1860-5397